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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Alabarse, Frederico
Elettra-Sincrotrone Trieste S.C.p.A.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2024Structural stability and adsorption behaviour of CO2-loaded pure silica CHA and ITW zeolites upon compressioncitations
- 2022Compressibility, Phase Transition, and Argon Insertion in the Siliceous Zeolite Mobil-Twelve at High Pressurecitations
- 2021High-Pressure Synthesis and Gas-Sensing Tests of 1-D Polymer/Aluminophosphate Nanocompositescitations
- 2021High-Pressure Synthesis and Gas-Sensing Tests of 1-D Polymer/Aluminophosphate Nanocompositescitations
- 2020Single-crystal diffraction at the high-pressure Indo-Italian beamline Xpress at Elettra, Triestecitations
- 2019Effect of H2O on the Pressure-Induced Amorphization of Hydrated AlPO4-17citations
- 2019Effect of H2O on the Pressure-Induced Amorphization of Hydrated AlPO4-17citations
- 2017Anomalous Compressibility and Amorphization in AlPO4-17, the Oxide with the Highest Negative Thermal Expansioncitations
- 2015AlPO4-54-AlPO4-8 Structural Phase Transition and Amorphization under High Pressurecitations
- 2014New experimental set-ups for studying nanoconfined water on the AILES beamline at SOLEILcitations
- 2014Effect of H2O on the Pressure-Induced Amorphization of AlPO4-54 center dot xH(2)Ocitations
Places of action
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article
Single-crystal diffraction at the high-pressure Indo-Italian beamline Xpress at Elettra, Trieste
Abstract
<jats:p>In this study the first <jats:italic>in situ</jats:italic> high-pressure single-crystal X-ray diffraction experiments at Xpress, the Indo-Italian beamline of the Elettra synchrotron, Trieste (Italy), are reported. A description of the beamline experimental setup and of the procedures for single-crystal centring, data collection and processing, using diamond anvil cells, are provided. High-pressure experiments on a synthetic crystal of clinoenstatite (MgSiO<jats:sub>3</jats:sub>), CaCO<jats:sub>3</jats:sub> polymorphs and a natural sample of leucophoenicite [Mn<jats:sub>7</jats:sub>Si<jats:sub>3</jats:sub>O<jats:sub>12</jats:sub>(OH)<jats:sub>2</jats:sub>] validated the suitability of the beamline experimental setup to: (i) locate and characterize pressure-induced phase transitions; (ii) solve <jats:italic>ab initio</jats:italic> the crystal structure of high-pressure polymorphs; (iii) perform fine structural analyses at the atomic scale as a function of pressure; (iv) disclose complex symmetry and structural features undetected using conventional X-ray sources.</jats:p>