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| Naji, M. |
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| Ertürk, Emre |
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| Azevedo, Nuno Monteiro |
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Cervellino, Antonio
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Publications (8/8 displayed)
- 2024Size- and temperature-dependent lattice anisotropy and structural distortion in CsPbBr 3 quantum dots by reciprocal space X-ray total scattering analysiscitations
- 2023Size‐ and Temperature‐Dependent Lattice Anisotropy and Structural Distortion in CsPbBr<sub>3</sub> Quantum Dots by Reciprocal Space X‐ray Total Scattering Analysiscitations
- 2022Competing phases in the room-temperature M 2 (2,6-ndc) 2 (dabco) metal-organic framework thin film synthesiscitations
- 2019Structural disorder and magnetic correlations driven by oxygen doping in Nd_{2}NiO_{4+δ} ( δ ∼ 0.11 )citations
- 2019A dilute gold nanoparticle suspension as small-angle X-ray scattering standard for an absolute scale using an extended Guinier approximationcitations
- 2018Size-dependent fault-driven relaxation and faceting in zincblende CdSe colloidal quantum dotscitations
- 2011Investigating the amorphous–crystalline interplay in SiO2/TiO2 nanocomposites by total scattering methodscitations
- 2001Ordering Principles in Decagonal Al-Co-Ni Quasicrystalscitations
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article
A dilute gold nanoparticle suspension as small-angle X-ray scattering standard for an absolute scale using an extended Guinier approximation
Abstract
<jats:p>In this article, a practical procedure for absolute intensity calibration for small-angle scattering (SAXS) studies on liquid microjets is established. A gold nanoparticle suspension is used as standard so that the intercept at <jats:italic>Q</jats:italic> = 0 of the SAXS scattering curve provides a scaling reference. In order to obtain the most precise extrapolation at <jats:italic>Q</jats:italic> = 0, an extension of the Guinier approximation has been used, with a second-order term in the fit that adapts to a larger <jats:italic>Q</jats:italic> range.</jats:p>