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Davies, John E.
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article
(η3-Allyl)[(S)-(+)-(2-pyrrolidinylmethyl)-pyrrolidine] palladium(II) trifluoromethane-sulfonate
Abstract
<p>The title compound, [Pd(C<sub>3</sub>H<sub>5</sub>)(C<sub>9</sub>H <sub>18</sub>N<sub>2</sub>)]CF<sub>3</sub>SO<sub>3</sub>, crystallizes in the non-centrosymmetric space group P2<sub>1</sub>2<sub>1</sub>2<sub>1</sub> and contains only one crystallographically unique Pd metal centre, showing a pseudo-square-planar geometry. (S)-(+)-(2-Pyrrolidinylmethyl)pyrrolidine (pmp, C<sub>9</sub>H<sub>18</sub>N<sub>2</sub>) acts as an N,N′-bidentate chelating ligand, leading to the formation of the chiral [Pd(η<sup>3</sup>- allyl)(pmp)]<sup>+</sup> complex cation, which is hydrogen bonded to the trifluoromethanesulfonate anion.</p>