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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Michalicka, Jan
Brno University of Technology
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2024Low‐Temperature Atomic Layer Deposition Synthesis of Vanadium Sulfide (Ultra)Thin Films for Nanotubular Supercapacitorscitations
- 2023Carboxymethyl starch as a reducing and capping agent in the hydrothermal synthesis of selenium nanostructures for use with three-dimensional-printed hydrogel carrierscitations
- 2022Hierarchical Atomic Layer Deposited V<sub>2</sub>O<sub>5</sub> on 3D Printed Nanocarbon Electrodes for High‐Performance Aqueous Zinc‐Ion Batteriescitations
- 2022Effect of Gd addition on the structural and magnetic properties of L1(0)-FePt alloy thin filmscitations
- 2021The Growth, Composition, and Functional Properties of Self‐Organized Nanostructured ZrO2‐Al2O3 Anodic Films for Advanced Dielectric Applicationscitations
- 2021Atomic layer deposition of photoelectrocatalytic material on 3D-printed nanocarbon structures ; Depozice atomárních vrstev fotoelektrokatalytického materiálu na 3D tištěné uhlíkové nanostruktury.citations
- 2020Laser-induced crystallization of anodic TiO2 nanotube layerscitations
- 2020Atomic Layer Deposition of MoSe2 Using New Selenium Precursors ; Depozice atomárních vrstev MoSe2 s použitím nových selenových prekurzorůcitations
- 2020Atomic Layer Deposition of MoSe2 Using New Selenium Precursorscitations
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article
Carboxymethyl starch as a reducing and capping agent in the hydrothermal synthesis of selenium nanostructures for use with three-dimensional-printed hydrogel carriers
Abstract
<jats:p>The hydrothermal method is a cost-effective and eco-friendly route for preparing various nanomaterials. It can use a capping agent, such as a polysaccharide, to govern and define the nanoparticle morphology. Elemental selenium nanostructures (spheres and rods) were synthesized and stabilized using a tailor-made carboxymethyl starch (CMS, degree of substitution = 0.3) under hydrothermal conditions. CMS is particularly convenient because it acts simultaneously as the capping and reducing agent, as verified by several analytical techniques, while the reaction relies entirely on green solvents. Furthermore, the effect of sodium selenite concentration, reaction time and temperature on the nanoparticle size, morphology, microstructure and chemical composition was investigated to identify the ideal synthesis conditions. A pilot experiment demonstrated the feasibility of implementing the synthesized nanoparticles into vat photopolymerization three-dimensional-printed hydrogel carriers based on 2-hydroxyethyl methacrylate (HEMA). When submersed into the water, the subsequent particle release was confirmed by dynamic light scattering (DLS), promising great potential for use in bio-three-dimensional printing and other biomedical applications.</jats:p>