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Kilian, Petr
University of St Andrews
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2021Synthetic and structural study of peri -substituted phosphine-arsinescitations
- 2021Synthetic and structural study of peri-substituted phosphine-arsinescitations
- 2021Synthetic and structural study of peri-substituted phosphine-arsinescitations
- 2019A study of through-space and through-bond JPP coupling in a rigid nonsymmetrical bis(phosphine) and its metal complexescitations
- 2018A study of through-space and through-bond JPP coupling in a rigid nonsymmetrical bis(phosphine) and its metal complexescitations
- 2018A study of through-space and through-bond J PP coupling in a rigid nonsymmetrical bis(phosphine) and its metal complexescitations
- 2016Varying the flexibility of the aromatic backbone in half sandwich rhodium(III) dithiolato complexes:a synthetic, spectroscopic and structural investigationcitations
- 2016Rhodium(III) and iridium(III) half-sandwich complexes with tertiary arsine and stibine ligandscitations
- 2016Varying the flexibility of the aromatic backbone in half sandwich rhodium(III) dithiolato complexescitations
- 2016Varying the flexibility of the aromatic backbone in half sandwich rhodium(III) dithiolato complexes : a synthetic, spectroscopic and structural investigationcitations
- 2015Rhodium(III) and iridium(III) half-sandwich complexes with tertiary arsine and stibine ligandscitations
- 2003Phosphorus-selenium heterocycles from the tetraphospholane (PhP) 4 CH 2
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article
Varying the flexibility of the aromatic backbone in half sandwich rhodium(III) dithiolato complexes
Abstract
A series of rhodium(III) half sandwich complexes of the type [Cp*Rh(PMe<sub>3</sub>)(S—R—S)]; S—R—S = naphthalene-1,8-dithiolate, acenaphthene-5,6-dithiolate, [1,1′-biphenyl]-2,2′-dithiolate and [2,2′-binaphthalene]-1,1′-dithiolate are reported. In the case of [2,2′-binaphthalene]-1,1′-dithiolate this represents an infrequent example of a metal complex containing this ligand. All the complexes have been fully characterised using multinuclear NMR spectroscopy and single crystal X-ray diffraction. The single crystal X-ray structure of the starting material [Cp*Rh(PMe<sub>3</sub>)Br<sub>2</sub>] (<b>1</b>) is also reported for the first time.