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Kowalska, E.
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article
Carbon-encapsulated magnetic nanoparticles spontaneously formed by thermolysis route
Abstract
<p>A new method for producing carbon-encapsulated magnetic nanoparticles using a thermolysis route is developed. The method is based on dechlorination of C6Cl6 with NaN3 in the presence of Fe or Fe14Nd2B magnetic alloy. The as-obtained products contained carbon-encapsulated magnetic nanoparticles with the diameters between 20 and 60 nm. The products were purified and their composition and morphology were studied by means of SEM, TEM, XRD and TG-DTA. The carbon-encapsulated nanoparticles are superparamagnetic with the maximum saturation magnetization of 20 emu/g. This autothermal process has inherent advantages, including the use of low cost materials and the simplicity of the production protocol.</p>