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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Calvo-Dahlborg, Monique
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (9/9 displayed)
- 2023Effect of Y2O3 addition on the microstructure and mechanical properties of an Al1.8CoCrCu0.5FeNi BCC HEAcitations
- 2021Investigation into the magnetic properties of CoFeNiCryCux alloyscitations
- 2021Design and production of a new feconicralcu high-entropy alloy: influence of powder production method on sinteringcitations
- 2021Design and Production of a New FeCoNiCrAlCu High-Entropy Alloy: Influence of Powder Production Method on Sinteringcitations
- 2016Structural and Microstructural Characterization of CoCrFeNiPd High Entropy Alloyscitations
- 2011Gas atomization of Al-Ni powders: Solidification modeling and neutron diffraction analysiscitations
- 2009Identification of phases in gas-atomised droplets by combination of neutron and X-ray diffraction techniques with atom probe tomographycitations
- 2003Amorphous alloy composition with high glass-formation ability in the pseudoternary Zr-[IQC-Al62Cu25.5Fe12.5]-[DQC-Al70Co15Ni15] alloy systemcitations
- 2002Synthesis of Cu47Ti34Zr11Ni8Bulk Metallic Glass by Warm Extrusion of Gas Atomized Powderscitations
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article
Identification of phases in gas-atomised droplets by combination of neutron and X-ray diffraction techniques with atom probe tomography
Abstract
Powders of Al68.5Ni31.5 alloy have been produced by gas atomisation and sieved in different grain size families. The resulting families have been analysed by combined neutron and X-ray diffraction in order to investigate the structure and identify the existing phases at the surface and in the bulk of the grains. The weight fraction of the identified phases (Al3Ni2, Al3Ni and Al) has been estimated from a profile refinement with the FULLPROF computer codes. An additional phase was observed but could not be identified in the diffraction patterns. Starting from grains less than 5 ??m in diameter, samples have been shaped by annular focused ion beam into needles that were suitable for atom probe investigations. The structure and morphologies observed by different techniques are compared and discussed. It has also been possible to estimate the crystallite sizes and the strains corresponding to the different phases present in the powders from the refinement of the ND patterns. In addition to Al3Ni2 and Al3Ni, a phase of composition close to the nominal one of the alloy was observed in the atom probe measurements. This phase could be one of the decagonal ones referred to in the literature. Small particles of composition close to Al82Ni18 are attributed to the metastable Al9Ni2 phase. The achieved conclusions demonstrate the complementarity of X-ray and neutron diffraction techniques and atom probe tomography to analyse complex structures. ?? 2008 Elsevier B.V. All rights reserved.