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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Larsson, Alfred
Lund University
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2024Dynamics of early-stage oxide formation on a Ni-Cr-Mo alloycitations
- 2023Understanding passive film degradation and its effect on hydrogen embrittlement of super duplex stainless steel-Synchrotron X-ray and electrochemical measurements combined with CalPhaD and ab-initio computational studiescitations
- 2023Ex‐situ synchrotron X‐ray diffraction study of CO2 corrosion‐induced surface scales developed in low‐alloy steel with different initial microstructurecitations
- 2023Ex‐situ synchrotron X‐ray diffraction study of CO2 corrosion‐induced surface scales developed in low‐alloy steel with different initial microstructurecitations
- 2023In situ quantitative analysis of electrochemical oxide film development on metal surfaces using ambient pressure X-ray photoelectron spectroscopy : Industrial alloyscitations
- 2023The causation of hydrogen embrittlement of duplex stainless steel : Phase instability of the austenite phase and ductile-to-brittle transition of the ferrite phase – Synergy between experiments and modellingcitations
- 2023The Causation of Hydrogen Embrittlement of Duplex Stainless Steel: Phase Instability of the Austenite Phase and Ductile-to-Brittle Transition of the Ferrite Phase – Synergy between Experiments and Modellingcitations
- 2023Understanding Passive Film Degradation and its Effect on Hydrogen Embrittlement of Super Duplex Stainless Steel – Synchrotron X-ray and Electrochemical Measurements combined with CalPhaD and ab-initio Computational Studiescitations
- 2023Synchrotron XPS and Electrochemical Study of Aging Effect on Passive Film of Ni Alloyscitations
- 2023Anisotropic strain variations during the confined growth of Au nanowirescitations
- 2022Thickness and composition of native oxides and near-surface regions of Ni superalloyscitations
- 2022Thickness and composition of native oxides and near-surface regions of Ni superalloyscitations
- 2021Operando Reflectance Microscopy on Polycrystalline Surfaces in Thermal Catalysis, Electrocatalysis, and Corrosioncitations
- 2020Metastable Precursor Structures in Hydrogen-infused Super Duplex Stainless Steel Microstructure – An Operando Diffraction Experimentcitations
- 2020Time-resolved Grazing-Incidence X-ray Diffraction Measurement to Understand the Effect of Hydrogen on Surface Strain Development in Super Duplex Stainless Steelcitations
Places of action
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article
Anisotropic strain variations during the confined growth of Au nanowires
Abstract
<jats:p>The electrochemical growth of Au nanowires in a template of nanoporous anodic aluminum oxide was investigated in situ by means of grazing-incidence transmission small- and wide-angle x-ray scattering (GTSAXS and GTWAXS), x-ray fluorescence (XRF), and two-dimensional surface optical reflectance. The XRF and the overall intensity of the GTWAXS patterns as a function of time were used to monitor the progress of the electrodeposition. Furthermore, we extracted powder diffraction patterns in the direction of growth and in the direction of confinement to follow the evolution of the direction-dependent strain. Quite rapidly after the beginning of the electrodeposition, the strain became tensile in the vertical direction and compressive in the horizontal direction, which showed that the lattice deformation of the nanostructures can be artificially varied by an appropriate choice of the deposition time. By alternating sequences of electrodeposition with sequences of rest, we observed fluctuations of the lattice parameter in the direction of growth, attributed to stress caused by electromigration. Furthermore, the porous domain size calculated from the GTSAXS patterns was used to monitor how homogeneously the pores were filled.</jats:p>