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Chmielewski, Adrian
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Topics
Publications (6/6 displayed)
- 2022Effect of size on the surface energy of noble metal nanoparticles from analytical and numerical approachescitations
- 2022Alloyed β-(Al<i>x</i>Ga1−<i>x</i>)2O3 bulk Czochralski single β-(Al0.1Ga0.9)2O3 and polycrystals β-(Al0.33Ga0.66)2O3, β-(Al0.5Ga0.5)2O3), and property trendscitations
- 2021Atomic-scale characterization of structural and electronic properties of Hf doped β-Ga2O3citations
- 2021Is There Really a Size effect on the Surface Energy of Nanoparticles ?
- 2018Direct Measurement of the Surface Energy of Bimetallic Nanoparticles: Evidence of Vegard’s Rulelike Dependencecitations
- 2017Direct measurement of the surface energy of bimetallic nanoparticles: Evidence of Vegard's rule-like dependencecitations
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article
Alloyed β-(Al<i>x</i>Ga1−<i>x</i>)2O3 bulk Czochralski single β-(Al0.1Ga0.9)2O3 and polycrystals β-(Al0.33Ga0.66)2O3, β-(Al0.5Ga0.5)2O3), and property trends
Abstract
<jats:p>In this work, bulk Czochralski-grown single crystals of 10 mol. % Al2O3 alloyed β-Ga2O3—monoclinic 10% AGO or β-(Al0.1Ga0.9)2O3—are obtained, which show +0.20 eV increase in the bandgap compared with unintentionally doped β-Ga2O3. Further, growths of 33% AGO—β-(Al0.33Ga0.67)2O3—and 50% AGO—β-(Al0.5Ga0.5)2O3 or β-AlGaO3—produce polycrystalline single-phase monoclinic material (β-AGO). All three compositions are investigated by x-ray diffraction, Raman spectroscopy, optical absorption, and 27Al nuclear magnetic resonance (NMR). By investigating single phase β-AGO over a large range of Al2O3 concentrations (10–50 mol. %), broad trends in the lattice parameter, vibrational modes, optical bandgap, and crystallographic site preference are determined. All lattice parameters show a linear trend with Al incorporation. According to NMR, aluminum incorporates on both crystallographic sites of β-Ga2O3, with a slight preference for the octahedral (GaII) site, which becomes more disordered with increasing Al. Single crystals of 10% AGO were also characterized by x-ray rocking curve, transmission electron microscopy, purity (glow discharge mass spectroscopy and x-ray fluorescence), optical transmission (200 nm–20 μm wavelengths), and resistivity. These measurements suggest that electrical compensation by impurity acceptor doping is not the likely explanation for high resistivity, but rather the shift of a hydrogen level from a shallow donor to a deep acceptor due to Al alloying. Bulk crystals of β-(Al0.1Ga0.9)2O3 have the potential to be ultra-wide bandgap substrates for thin film growth, with a lattice parameter that may even allow higher Al concentration β-Ga2O3 single crystal thin films to be grown.</jats:p>