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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Van Breemen, Lambèrt C. A.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (34/34 displayed)
- 2024A macroscopic viscoelastic viscoplastic constitutive model for porous polymers under multiaxial loading conditionscitations
- 2024Vezel-geïnduceerde kristallisatie in rekstromingen ; Fiber-induced crystallization in elongational flowscitations
- 2024Fiber-induced crystallization in elongational flowscitations
- 2023Deformation kinetics of single-fiber polypropylene composites:Adhesion improvement at the expense of toughness
- 2023Deformation kinetics of single-fiber polypropylene composites
- 2023Shear-Induced Structure Formation in MAH-g-PP Compatibilized Polypropylenescitations
- 2022In Situ Fabrication, Manipulation, and Mechanical Characterization of Free-Standing Silica Thin Films Using Focused Ion Beam Scanning Electron Microscopycitations
- 2022In Situ Fabrication, Manipulation, and Mechanical Characterization of Free-Standing Silica Thin Films Using Focused Ion Beam Scanning Electron Microscopycitations
- 2022Laser sintering of PA12 particles studied by in-situ optical, thermal and X-ray characterizationcitations
- 2020Polarization modulated infrared spectroscopy:A pragmatic tool for polymer science and engineeringcitations
- 2020Polymer spheres
- 2020Polarization modulated infrared spectroscopycitations
- 2020Transient dynamics of cold-rolled and subsequently thermally rejuvenated atactic-polystyrene using broadband dielectric spectroscopycitations
- 2020Thermally Reversible Diels–Alder Bond-Containing Acrylate Networks Showing Improved Lifetimecitations
- 2020Thermally Reversible Diels–Alder Bond-Containing Acrylate Networks Showing Improved Lifetimecitations
- 2019Predicting embrittlement of polymer glasses using a hydrostatic stress criterioncitations
- 2019Hydrostatic stress as indicator for wear initiation in polymer tribologycitations
- 2019Effect of low-temperature physical aging on the dynamic transitions of atactic polystyrene in the glassy statecitations
- 2019A novel experimental setup for in-situ optical and X-ray imaging of laser sintering of polymer particlescitations
- 2019Temperature dependent two-body abrasive wear of polycarbonate surfacescitations
- 2019Laser sintering of polymer particle pairs studied by in-situ visualizationcitations
- 2018Contact mechanics of high-density polyethylene: Effect of pre-stretch on the frictional response and the onset of wearcitations
- 2018Thin film mechanical characterization of UV-curing acrylate systemscitations
- 2018Contact mechanics of polyolefins: effect of pre-stretch on the frictional response and the onset of wear
- 2017Experimental setup for in situ visualization studies of laser sintering of polymer particles
- 2011Criteria to predict the embrittlement of polycarbonatecitations
- 2011Extending the EGP constitutive model for polymer glasses to multiple relaxation timescitations
- 2009Predicting the long-term mechanical performance of polycarbonate from thermal history during injection moldingcitations
- 2009Predicting the yield stress of polymer glasses directly from processing conditions: application to miscible systemscitations
- 2009Numerical simulation of flat-tip micro-indentation of glassy polymers: influence of loading speed and thermodynamic statecitations
- 2006Indentation: the experimenter's holy grail for small-scale polymer characterization?
- 2006Modelling large-strain deformation of thermo-rheologically complex materials : characterisation and validation of PMMA and iPP
- 2005Quantitative prediction of long-term failure of Polycarbonatecitations
- 2004Structure, deformation, and failure of flow-oriented semicrystalline polymerscitations
Places of action
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article
A novel experimental setup for in-situ optical and X-ray imaging of laser sintering of polymer particles
Abstract
We present a unique laser sintering setup that allows real time studies of the structural evolution during laser sintering of polymer particles. The device incorporates the main features of classical selective laser sintering machines for 3D printing of polymers and at the same time allows in situ visualization of the sintering dynamics with optical microscopy as well as X-ray scattering. A main feature of the setup is the fact that it provides local access to one particle-particle bridge during sintering. In addition, due to the small scale of the device and the specific laser arrangement process, parameters such as the temperature, laser energy, laser pulse duration, and spot size can be precisely controlled. The sample chamber provides heating up to 360 °C, which allows for sintering of commodity as well as high performance polymers. The latter parameters are controlled by the use of a visible light laser combined with an acousto-optic modulator for pulsing, which allows small and precise spot sizes and pulse times and pulse energies as low as 500 μs and 17 μJ. The macrostructural evolution of the particle bridge during sintering is followed via optical imaging at high speed and resolution. Placing the setup in high flux synchrotron radiation with a fast detector simultaneously allows in situ time-resolved X-ray characterizations. To demonstrate the capabilities of the device, we studied the laser sintering of two spherical PA12 particles. The setup provides crucial real-time information concerning the sintering dynamics as well as crystallization kinetics, which was not accessible up to now.