| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Mangler, Clemens
University of Vienna
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2024Grain-Size-Dependent Plastic Behavior in Bulk Nanocrystalline FeAl
- 2023Interface effects on titanium growth on graphenecitations
- 2023Creation of Single Vacancies in hBN with Electron Irradiationcitations
- 2021The morphology of doubly-clamped graphene nanoribbons
- 2014Nitrogen controlled iron catalyst phase during carbon nanotube growthcitations
- 2012Radiation effects in bulk nanocrystalline FeAl alloycitations
- 2012Spinodal decomposition in (CaxBa1-x)(y)Fe4Sb12citations
- 2011Growth of nanosized chemically ordered domains in intermetallic FeAl made nanocrystalline by severe plastic deformationcitations
- 2011Three-Dimensional Analysis by Electron Diffraction Methods of Nanocrystalline Materialscitations
- 2011Thermally induced transition from a ferromagnetic to a paramagnetic state in nanocrystalline FeAl processed by high-pressure torsioncitations
- 2010Electron microscopy of severely deformed L12 intermetallicscitations
- 2010Quantitative local profile analysis of nanomaterials by electron diffractioncitations
- 2010Structural modifications during heating of bulk nanocrystalline FeAl produced by high-pressure torsioncitations
- 2008TEM study of local disordering: a structural phase change induced by high-pressure torsioncitations
- 2004Nanostructures in L12-ordered Cu3Au processed by torsion under high pressurecitations
Places of action
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article
Nitrogen controlled iron catalyst phase during carbon nanotube growth
Abstract
Close control over the active catalyst phase and hence carbon nanotube structure remains challenging in catalytic chemical vapor deposition since multiple competing active catalyst phases typically co-exist under realistic synthesis conditions. Here, using in-situ X-ray diffractometry, we show that the phase of supported iron catalyst particles can be reliably controlled via the addition of NH3 during nanotube synthesis. Unlike polydisperse catalyst phase mixtures during H2 diluted nanotube growth, nitrogen addition controllably leads to phase-pure γ-Fe during pre-treatment and to phase-pure Fe3C during growth. We rationalize these findings in the context of ternary Fe-C-N phase diagram calculations and, thus, highlight the use of pre-treatment- and add-gases as a key parameter towards controlled carbon nanotube growth.