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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Felici, R.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2023Spin-dependent charge transmission through chiral 2T3N self-assembled monolayer on Aucitations
- 2019Emerging proton conductivity at the interface between insulating NdGa O3 and BaZr O3citations
- 2019Regular Network of Misfit Dislocations at the BaZr 0.8 Y 0.2 O 3−x /NdGaO 3 Interface and Its Role in Proton Conductivitycitations
- 2018Al5Co2 intermetallic compounds as catalysts for hydrogenation: surface structure and reactivity
- 2014Synthesis and Technological Application of Electrodeposited Semiconductors by EC-ALD
- 2014An in situ and ex situ SXRD and TEM microscopy study of CuXSZ and CuXZnYSZ thin films
- 2013Measurement of the effect of lattice strain on magnetic interactions and orbital splitting in CaCuO2 using resonant inelastic x-ray scatteringcitations
- 2012Surface X-ray diffraction analysis of Fe nanostructured films grown on c(2×2)-N/Cu(100)citations
- 2010Ultrahigh vacuum/high-pressure flow reactor for surface x-ray diffraction and grazing incidence small angle x-ray scattering studies close to conditions for industrial catalysiscitations
- 2005Upper critical fields up to 60 T in dirty magnesium diboride thin filmscitations
- 2004Epitaxial MgB2 thin films on ZrB2 buffer layers: structural characterization by synchrotron radiationcitations
- 2002Anisotropy in c-oriented MgB2 thin films grown by pulsed laser depositioncitations
- 2001Growth of c-oriented MgB2 thin films by pulsed laser deposition: structural characterization and electronic anisotropycitations
- 2000Strain-driven transition from stepped interfaces to regularly spaced macrosteps in (GaIn)As/Ga(PAs) symmetrically strained superlatticescitations
Places of action
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article
Ultrahigh vacuum/high-pressure flow reactor for surface x-ray diffraction and grazing incidence small angle x-ray scattering studies close to conditions for industrial catalysis
Abstract
<p>A versatile instrument for the in situ study of catalyst surfaces by surface x-ray diffraction and grazing incidence small angle x-ray scattering in a 13 ml flow reactor combined with reaction product analysis by mass spectrometry has been developed. The instrument bridges the so-called "pressure gap" and "materials gap" at the same time, within one experimental setup. It allows for the preparation and study of catalytically active single crystal surfaces and is also equipped with an evaporator for the deposition of thin, pure metal films, necessary for the formation of small metal particles on oxide supports. Reactions can be studied in flow mode and batch mode in a pressure range of 100-1200 mbar and temperatures up to 950 K. The setup provides a unique combination of sample preparation, characterization, and in situ experiments where the structure and reactivity of both single crystals and supported nanoparticles can be simultaneously determined.</p>