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Castillo-Blas, Celia
University of Cambridge
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (16/16 displayed)
- 2024Synthetic and analytical considerations for the preparation of amorphous metal-organic frameworks.
- 2024Transient intermediate in the formation of an amorphous metal-organic framework.
- 2024Structural insights into hybrid immiscible blends of metal-organic framework and sodium ultraphosphate glasses
- 2024Transient intermediate in the formation of an amorphous metal-organic frameworkcitations
- 2024Mechanochemically-induced glass formation from two-dimensional hybrid organic-inorganic perovskites.
- 2024Mechanochemically-induced glass formation from two-dimensional hybrid organic–inorganic perovskitescitations
- 2024Mechanochemically-induced glass formation from two-dimensional hybrid organic–inorganic perovskitescitations
- 2023Interfacial Bonding between a Crystalline Metal-Organic Framework and an Inorganic Glasscitations
- 2023Structural insights into hybrid immiscible blends of metal-organic framework and sodium ultraphosphate glasses.
- 2023Interfacial Bonding between a Crystalline Metal-Organic Framework and an Inorganic Glass.
- 2023Structural insights into hybrid immiscible blends of metal–organic framework and sodium ultraphosphate glassescitations
- 2022Principles of melting in hybrid organic-inorganic perovskite and polymorphic ABX3 structures.
- 2022Materials Formed by Combining Inorganic Glasses and Metal-Organic Frameworks.
- 2020The role of defects in the properties of functional coordination polymerscitations
- 2020Unravelling the local structure of catalytic Fe-oxo clusters stabilized on the MOF-808 metal organic-frameworkcitations
- 2016Crystal phase competition by addition of a second metal cation in solid solution metal–organic frameworkscitations
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article
Transient intermediate in the formation of an amorphous metal-organic framework
Abstract
<p>Amorphous metal-organic frameworks are rarely formed via direct synthesis. Our limited understanding of their atomic assembly in solution prevents full exploitation of their unique structural complexity. Here, we use in situ synchrotron X-ray absorption spectroscopy with sub-second time resolution to probe the formation of the amorphous Fe-BTC framework. Using a combination of spectral fingerprinting, linear combination analysis, and principal component analysis coupled with kinetic analyses, we reveal a multi-stage formation mechanism that, crucially, proceeds via the generation of a transient intermediate species.</p>