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Keenan, Luke
Diamond Light Source
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Publications (4/4 displayed)
- 2024Transient intermediate in the formation of an amorphous metal-organic framework.
- 2024Transient intermediate in the formation of an amorphous metal-organic frameworkcitations
- 2021Structural Evolution of Iron Forming Iron Oxide in a Deep Eutectic-Solvothermal Reactioncitations
- 2021Photon-in/photon-out spectroscopy at the I20-scanning beamline at diamond light sourcecitations
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article
Transient intermediate in the formation of an amorphous metal-organic framework
Abstract
<p>Amorphous metal-organic frameworks are rarely formed via direct synthesis. Our limited understanding of their atomic assembly in solution prevents full exploitation of their unique structural complexity. Here, we use in situ synchrotron X-ray absorption spectroscopy with sub-second time resolution to probe the formation of the amorphous Fe-BTC framework. Using a combination of spectral fingerprinting, linear combination analysis, and principal component analysis coupled with kinetic analyses, we reveal a multi-stage formation mechanism that, crucially, proceeds via the generation of a transient intermediate species.</p>