693.932 PEOPLE
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| Naji, M. |
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| Ertürk, Emre |
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| Petrov, R. H. | Madrid |
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| Casati, R. |
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| Azevedo, Nuno Monteiro |
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Sapnik, Af
University of Copenhagen
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2024Transient intermediate in the formation of an amorphous metal-organic frameworkcitations
- 2023Interfacial Bonding between a Crystalline Metal-Organic Framework and an Inorganic Glasscitations
- 2023Mapping nanocrystalline disorder within an amorphous metal–organic frameworkcitations
- 2023Structural insights into hybrid immiscible blends of metal–organic framework and sodium ultraphosphate glassescitations
- 2022Modeling the Effect of Defects and Disorder in Amorphous Metal-Organic Frameworkscitations
- 2021Melting of hybrid organic–inorganic perovskitescitations
- 2021Stepwise collapse of a giant pore metal-organic frameworkcitations
- 2021Mixed hierarchical local structure in a disordered metal–organic frameworkcitations
- 2020A new route to porous metal-organic framework crystal-glass compositescitations
- 2018Compositional inhomogeneity and tuneable thermal expansion in mixed-metal ZIF-8 analoguescitations
- 2018Uniaxial negative thermal expansion and metallophilicity in Cu3[Co(CN)6]citations
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article
Transient intermediate in the formation of an amorphous metal-organic framework
Abstract
<p>Amorphous metal-organic frameworks are rarely formed via direct synthesis. Our limited understanding of their atomic assembly in solution prevents full exploitation of their unique structural complexity. Here, we use in situ synchrotron X-ray absorption spectroscopy with sub-second time resolution to probe the formation of the amorphous Fe-BTC framework. Using a combination of spectral fingerprinting, linear combination analysis, and principal component analysis coupled with kinetic analyses, we reveal a multi-stage formation mechanism that, crucially, proceeds via the generation of a transient intermediate species.</p>