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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Hall, Simon R.
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Publications (8/8 displayed)
- 2022Synthesis of porous high-temperature superconductors via a melamine formaldehyde sacrificial templatecitations
- 2021Facile synthesis of five strontium niobate metastable crystal compositions via sol-gel ionic liquid synthesiscitations
- 2020Metastable Crystalline Phase Formation in Deep Eutectic Systems Revealed by Simultaneous Synchrotron XRD and DSCcitations
- 2015On the Mechanism of Cuprate Crystal Growth:The Role of Mixed Metal Carbonatescitations
- 2014In Situ TEM Observation of a Microcrucible Mechanism of Nanowire Growthcitations
- 2013Designed 3D architectures of high-temperature superconductorscitations
- 2012Strain and architecture-tuned reactivity in ceria nanostructures; Enhanced catalytic oxidation of CO to CO2citations
- 2012High J(c) in a biopolymer-mediated synthesis of YBa2Cu3O7-deltacitations
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article
Synthesis of porous high-temperature superconductors via a melamine formaldehyde sacrificial template
Abstract
<p>Nanostructured high-temperature superconductors YBa<sub>2</sub>Cu<sub>3</sub>O<sub>6+δ</sub> and Bi<sub>2</sub>Sr<sub>2</sub>CaCu<sub>2</sub>O<sub>8+δ</sub> were synthesised using a melamine formaldehyde sponge as a sacrificial template, via three solution-based approaches. In the case of YBa<sub>2</sub>Cu<sub>3</sub>O<sub>6+δ</sub>, a modified Pechini method produced a material with a superconducting transition at 92 K and a specific surface area of 4.22 m<sup>2</sup> g<sup>−1</sup>. Further analysis with Hg porosimetry determined that the sponge exhibited a porosity of 82%. In the case of Bi<sub>2</sub>Sr<sub>2</sub>CaCu<sub>2</sub>O<sub>8+δ</sub>, this method produced a material that exhibited superconductivity at 86 K with a specific surface area of 9.62 m<sup>2</sup> g<sup>−1</sup>. Hg-porosimetry determined that the BSCCO sponge exhibited a porosity of 78%.</p>