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Clark, James Hanley
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Topics
Publications (10/10 displayed)
- 2020Deep Eutectic Solvents Based on Natural Ascorbic Acid Analogues and Choline Chloridecitations
- 2019Fabrication of PES/PVP Water Filtration Membranes Using Cyrene®, a Safer Bio-Based Polar Aprotic Solventcitations
- 2018Elucidating enzymatic polymerisationscitations
- 2017Wholly biomass derivable sustainable polymers by ring-opening metathesis polymerisation of monomers obtained from furfuryl alcohol and itaconic anhydridecitations
- 20172,2,5,5-Tetramethyltetrahydrofuran (TMTHF)citations
- 2016Ring opening metathesis polymerisation of a new bio-derived monomer from itaconic anhydride and furfuryl alcoholcitations
- 2015Bio-derived materials as a green route for precious & critical metal recovery and re-usecitations
- 2015New insights into the curing of epoxidized linseed oil with dicarboxylic acidscitations
- 2014Bio-based thermoset composites from epoxidised linseed oil and expanded starchcitations
- 2013Alkali silicates and structured mesoporous silicas from biomass power station waste: the emergence of bio-MCMscitations
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article
Wholly biomass derivable sustainable polymers by ring-opening metathesis polymerisation of monomers obtained from furfuryl alcohol and itaconic anhydride
Abstract
Ring-opening metathesis polymerisation (ROMP) of oxanorbornene esters by Grubbs second generation catalyst is used to prepare a range of wholly biomass-derivable homo and copolymers. Eight ester monomers are prepared by esterification of the corresponding carboxylic acid which itself is formed by a 100% atom-economical tandem Diels-Alder-lactonisation reaction ofitaconic anhydride and furfuryl alcohol. The well-controlled nature of the ROMP is confirmed by NMR studies and facilitated the preparation of homopolymers, random copolymers and block copolymers with good control over the polymer molecular weight and molecular weight distribution.