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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Styles, Mark J.
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Publications (5/5 displayed)
- 2017Fe3O4@HKUST-1 and Pd/Fe3O4@HKUST-1 as magnetically recyclable catalysts prepared via conversion from a Cu-based ceramiccitations
- 2015Positioning of the HKUST-1 metal-organic framework (Cu3(BTC)2) through conversion from insoluble Cu-based precursorscitations
- 2015Lead(II) uptake by aluminium based magnetic framework composites (MFCs) in watercitations
- 2015ZnO as an efficient nucleating agent for rapid, room temperature synthesis and patterning of Zn-based metal-organic frameworkscitations
- 2015Biomimetic mineralization of metal-organic frameworks as protective coatings for biomacromoleculescitations
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article
Fe3O4@HKUST-1 and Pd/Fe3O4@HKUST-1 as magnetically recyclable catalysts prepared via conversion from a Cu-based ceramic
Abstract
<p>Nanocomposites obtained by integrating iron oxide magnetic nanoparticles (Fe<sub>3</sub>O<sub>4</sub>) into a metal-organic framework (HKUST-1 or Cu<sub>3</sub>(BTC)<sub>2</sub>, BTC = 1,3,5-benzenetricarboxylate) are synthesized through conversion from a composite of a Cu-based ceramic material and Fe<sub>3</sub>O<sub>4</sub>. In situ small-angle X-ray scattering (SAXS) and wide-angle X-ray scattering (WAXS) measurements reveal that the presence of Fe<sub>3</sub>O<sub>4</sub> leads to the fast conversion and synthesis of HKUST-1 with small particle sizes. The prepared MOF composite (Fe<sub>3</sub>O<sub>4</sub>@HKUST-1) is found to catalyze the one-pot sequential deacetalization-Knoevenagel condensation reaction as a magnetically collectable and recyclable catalyst. In addition, Pd nanoparticles are also incorporated into the material (Pd/Fe<sub>3</sub>O<sub>4</sub>@HKUST-1) by addition of a Pd colloidal solution during the conversion of the precursor composite to HKUST-1. The resulting Pd/Fe<sub>3</sub>O<sub>4</sub>@HKUST-1 can be utilized for hydrogenation of 1-octene in the liquid phase.</p>