| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Biswas, K.
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (13/13 displayed)
- 2023Understanding the evolution of catalytically active multi-metal sites in a bifunctional high-entropy alloy electrocatalyst for zinc–air battery applicationcitations
- 2023Steering Large Magnetic Exchange Coupling in Nanographenes near the Closed-Shell to Open-Shell Transitioncitations
- 2022Texture Evolution During Hot Compression of CoCuFeMnNi Complex Concentrated Alloy Using Neutron Diffraction and Crystal Plasticity Simulationscitations
- 2021Easy scalable avenue of anti-bacterial nanocomposites coating containing Ag NPs prepared by cryomillingcitations
- 2021A Perspective on the Catalysis Using the High Entropy Alloyscitations
- 2021Low-cost high entropy alloy (HEA) for high-efficiency oxygen evolution reaction (OER)citations
- 2018Preparation of nanocrystalline high-entropy alloys via cryomilling of cast ingotscitations
- 2018Effect of Al Addition on the Microstructural Evolution of Equiatomic CoCrFeMnNi Alloycitations
- 2016Green synthesis of Ag nanoparticles in large quantity by cryomillingcitations
- 2006Fabrication of bulk amorphous Fe<inf>67</inf>Co<inf>9.5</inf>Nd <inf>3</inf>Dy<inf>0.5</inf>B<inf>20</inf> alloy by hot extrusion of ribbon and study of the magnetic propertiescitations
- 2006Glass-forming ability and fragility parameter of amorphous Fe <inf>67</inf>Co<inf>9.5</inf>Nd<inf>3</inf>Dy<inf>0.5</inf>B<inf>20</inf>citations
- 2006On the fragility of Cu<inf>47</inf>Ti<inf>33</inf>Zr<inf>11</inf>Ni <inf>8</inf>Si<inf>1</inf> metallic glasscitations
- 2005Crystallization kinetics of amorphous Fe<inf>67</inf>Co <inf>9.5</inf>Nd<inf>3</inf>Dy<inf>0.5</inf>B<inf>20</inf>citations
Places of action
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article
Green synthesis of Ag nanoparticles in large quantity by cryomilling
Abstract
Most of the synthetic methods for the preparation of Ag nanoparticles (Ag NPs) involve wet chemical synthesis, in which hazardous chemicals are used and the NPs are further stabilized by a surfactant. The presence of a surfactant is detrimental to the purity as well as to the native properties of the Ag NPs. The present study reports a unique technique to prepare ultrapure free-standing Ag NPs in large quantities without the use of any hazardous chemicals. This has been achieved by cryomilling. Note that cryomilling is a cost effective method to prepare metal NPs, involving ball milling below 160 ± 10 °C under a protective Ar atmosphere. The experimental results reveal that it is possible to obtain Ag NPs with a narrow size distribution (4–8 nm). The level of contamination (34 ppb of W) in the nanoparticles was estimated by EPMA, whereas the ultra-high purity of the Ag NPs was confirmed by ICP-OES and XPS. The surfactant-free Ag NPs were also stable at elevated temperatures (400 °C) and exhibited free-standing nature in liquids including ethanol, methanol, and water. The results have been discussed based on the low-temperature deformation behaviour of Ag and the electrostatic stabilization of highly pure Ag NPs in different polar liquids.