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Publications (4/4 displayed)
- 2022On the Fabrication of Defect-Free Nickel-Rich Nickel–Titanium Parts Using Laser Powder Bed Fusioncitations
- 2018Thermal conductivity in self-assembled CoFe2O4/BiFeO3 vertical nanocomposite filmscitations
- 2017Solventless mechanochemical metallation of porphyrinscitations
- 2017A Flexible and Efficient Output File Format for Grain-Scale Multiphysics Simulationscitations
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article
Solventless mechanochemical metallation of porphyrins
Abstract
A fast solvent-free method for the metallation of porphyrins is presented. ZnTPP, NiTPP, CuTPP and FeTPP have been prepared mechanochemically by ball milling hydrated metal acetate salts with meso-tetraphenylporphyrin (H2TPP) in a shaker mill for as little as 20 min with no added solvent, avoiding the need for undesirable solvents and long reaction times normally used in such reactions.