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Webster, Ruth
University of Cambridge
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (4/4 displayed)
- 2023The Complex Reactivity of [(salen)Fe]2(μ-O) with HBpin and its Implications in Catalysiscitations
- 2015Titanium pyridonates for the homo- and copolymerization of rac-lactide and ε-caprolactonecitations
- 2014Random copolymerisations catalysed by simple titanium α-amino acid complexescitations
- 2013Titanium pyridonates and amidates: novel catalysts for the synthesis of random copolymerscitations
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article
Titanium pyridonates for the homo- and copolymerization of rac-lactide and ε-caprolactone
Abstract
A series of titanium pyridonate complexes have been synthesized under very mild reaction conditions from a common precursor, Ti(NMe2)4. These complexes have been explored as initiators for the ring-opening polymerization of rac-lactide and ε-caprolactone and have proven to be competitive with leading titanium initiators. Furthermore, these complexes have been shown to be competent initiators for the synthesis of copolymers (CL–LA block copolymers and random copolymers). Metal complex reactivity trends in both homo- and copolymerization show that poly(lactic acid) is most susceptible to chain scission and transesterification.