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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Bourgeois, Laure
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Topics
Publications (8/8 displayed)
- 2021Dual Photolytic Pathways in an Alloyed Plasmonic Near-perfect Absorber: Implications for Photoelectrocatalysiscitations
- 2017The bi-layered precipitate phase ζ in the Al-Ag alloy systemcitations
- 2017The enhanced theta-prime (θ′) precipitation in an Al-Cu alloy with trace Au additionscitations
- 2014Particle evolution in Mg-Zn-Zr alloy processed by integrated extrusion and equal channel angular pressingcitations
- 2012A simple route to full structural analysis of biophosphates and their application to materials discoverycitations
- 2011Quantitative microscopic measurement of void distribution in shear bands in Zr(66.7)Cu(33.3) metallic glasscitations
- 2011High surface area templated LiFePO4 from a single source precursor moleculecitations
- 2002Boron nitride nanotube, nanocable and nanoconecitations
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article
A simple route to full structural analysis of biophosphates and their application to materials discovery
Abstract
An integrated suite of synthesis and characterisation techniques that includes synchrotron-based single crystal, powder X-Ray diffraction, nuclear magnetic resonance and electron diffraction have been employed to uncover two new distinct structures in the CaxBa2-xP2O7 polymorphic phosphate 10 system. These materials have particular relevance for their application as both biomaterials and phosphors. Calcium Barium Pyrophosphate, CaBaP2O7, was shown by a combination of spectroscopic and diffraction techniques to have two polymorphs distinct in structure from all of the five previously reported polymorphs of Ca, Sr and Ba Pyrophosphate . A high temperature polymorph HT-CaBaP2O7 prepared at 1200 ºC is orthorhombic of space group P212121 with a=13.0494 Å, b=8.9677 Å, c=5.5444 Å. A low temperature polymorph LT-CaBaP2O7, prepared below 1000 ºC, is monoclinic with space group P21/c and dimensions a=12.065 Å, b=10.582 Å, c=9.515 Å, β=94.609°.