Materials Map

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The Materials Map is an open tool for improving networking and interdisciplinary exchange within materials research. It enables cross-database search for cooperation and network partners and discovering of the research landscape.

The dashboard provides detailed information about the selected scientist, e.g. publications. The dashboard can be filtered and shows the relationship to co-authors in different diagrams. In addition, a link is provided to find contact information.

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The Materials Map is still under development. In its current state, it is only based on one single data source and, thus, incomplete and contains duplicates. We are working on incorporating new open data sources like ORCID to improve the quality and the timeliness of our data. We will update Materials Map as soon as possible and kindly ask for your patience.

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Naji, M.
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Brechin, Euan K.

  • Google
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University of Edinburgh

in Cooperation with on an Cooperation-Score of 37%

Topics

Publications (21/21 displayed)

  • 2025Robust Y and Lu TrenSal catalysts for ring-opening polymerisationcitations
  • 2021Oxidation state variation in bis-calix[4]arene supported decametallic Mn clusters2citations
  • 2020With complements of the ligands: an unusual S-shaped [Mn7]2 assembly from tethered calixarenes5citations
  • 2020Putting the squeeze on molecule-based magnets: exploiting pressure to develop magneto-structural correlations in paramagnetic coordination compounds10citations
  • 2019Effect of pi-aromatic spacers on the magnetic properties and slow relaxation of double stranded metallacyclophanes with a Ln(III)-M-II-M-II-Ln(III) (Ln(III) = Gd-III, Dy-III, Y-III; M-II = Ni-II, Co-II) linear topology9citations
  • 2019Molecular multifunctionality preservation upon surface deposition for a chiral single-molecule magnet23citations
  • 2018Order in disorder:solution and solid-state studies of [MM] wheels (M = Cr, Al; M = Ni, Zn)13citations
  • 2018Order in disorder: solution and solid-state studies of [MIII 2 MII 5] wheels (MIII = Cr, Al; MII = Ni, Zn)13citations
  • 2018Order in disorder13citations
  • 2010MCD spectroscopy of hexanuclear Mn(III) salicylaldoxime single-molecule magnets20citations
  • 2010Pressure-Induced Jahn-Teller Switching in a Mn12 nanomagnet57citations
  • 2010High pressure studies of hydroxo-bridged Cu(II) dimers26citations
  • 2010The effect of pressure on the crystal structure of [Gd(PhCOO) 3(DMF)]n to 3.7 GPa and the transition to a second phase at 5.0 GPa10citations
  • 2010The effect of pressure on the crystal structure of [Gd(PhCOO)(3)(DMF)](n) to 3.7 GPa and the transition to a second phase at 5.0 GPa10citations
  • 2009High pressure induced spin changes and magneto-structural correlations in hexametallic SMMs51citations
  • 2008Grafting derivatives of Mn-6 single-molecule magnets with high anisotropy energy barrier on Au(111) surface34citations
  • 2005Magnetic and theoretical characterization of a ferromagnetic Mn(III) dimer29citations
  • 2005Studies of an enneanuclear manganese single-molecule magnet93citations
  • 2004Synthesis, structure, and magnetic properties of a [Mn22] wheel-like single-molecule magnet147citations
  • 2004New routes to polymetallic clusters: Fluoride-based tri-, deca-, and hexaicosametallic MnIII clusters and their magnetic properties109citations
  • 2004New routes to polymetallic clusters109citations

Places of action

Chart of shared publication
Nichol, Gary S.
4 / 4 shared
Fazekas, Eszter
1 / 1 shared
Etcheverry-Berrios, Alvaro
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Piligkos, Stergios
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Garden, Jennifer A.
1 / 3 shared
Rajaraman, Gopalan
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Dalgarno, Scott J.
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Coletta, Marco
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Jose, Reshma
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Wilson, Lucinda R. B.
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Sanz, Sergio
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Parsons, Simon
5 / 10 shared
Murrie, Mark
5 / 6 shared
Moggach, Stephen A.
4 / 13 shared
Probert, Michael R.
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Kamenev, Konstantin V.
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Meseguer, Carlos
1 / 1 shared
Palacios, Maria A.
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Drahos, Bohuslav
1 / 1 shared
Colacio, Enrique
1 / 2 shared
Mota, Antonio J.
1 / 2 shared
Moreno, Jose M.
1 / 1 shared
Navarrete, R.
1 / 1 shared
Reinholdt, Anders
1 / 3 shared
Mitcov, Dmitri
1 / 3 shared
Wilhelm, Fabrice
1 / 29 shared
Hassenkam, Tue
1 / 3 shared
Gelardi, Rikke Munch
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Thulstrup, Peter Waaben
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Rogalev, Andrei
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Wernsdorfer, Wolfgang
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Konstantatos, Andreas
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Pedersen, Anders H.
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Vinum, Morten Gotthold
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Sørensen, Mikkel Agerbæk
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Ceccato, Marcel
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Evangelisti, Marco
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Uhrín, Dušan
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Nielsen, Ulla Gro
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Schnack, Jürgen
3 / 4 shared
Fraser, Hector W. L.
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Gro Nielsen, Ulla
1 / 1 shared
Milios, Constantinos J.
2 / 2 shared
Thomson, Andrew J.
1 / 2 shared
Inglis, Ross
1 / 1 shared
Bradley, Justin M.
1 / 2 shared
Kamenev, Konstantin K.
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Sanchez-Benitez, Javier
3 / 5 shared
Moggach, S. A.
1 / 1 shared
Lennie, A. R.
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Warren, J. E.
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Parois, P.
1 / 1 shared
Parsons, S.
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Murrie, M.
1 / 1 shared
Prescimone, Alessandro
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Warren, John E.
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Lennie, Alistair R.
4 / 5 shared
Parois, Pascal
2 / 3 shared
Kortus, Jens
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Loose, Claudia
1 / 1 shared
Moggach, Stephen
1 / 7 shared
Biagi, R.
1 / 2 shared
Milios, C. J.
1 / 1 shared
Pennino, U. Del
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Corradini, V.
1 / 3 shared
Jones, L. F.
2 / 2 shared
Evangelisti, M.
1 / 1 shared
Moro, F.
1 / 2 shared
Renzi, V. De
1 / 1 shared
Piligkos, S.
2 / 2 shared
Wernsdorfer, W.
4 / 6 shared
Sanudo, E. C.
2 / 2 shared
Helliwell, M.
1 / 4 shared
Christou, G.
4 / 5 shared
Rajaraman, G.
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Soler, M.
1 / 3 shared
Slageren, J. Van
1 / 1 shared
Kirchner, N.
1 / 1 shared
Gudel, H. U.
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Bircher, R.
1 / 1 shared
Kortus, J.
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Murugesu, M.
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Raftery, J.
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Teat, Simon J.
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Sanudo, E. Carolina
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Brockman, Jonathon
1 / 1 shared
Christou, George
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Murugesu, Muralee
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Jones, Leigh F.
1 / 1 shared
Collison, David
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Raftery, Jim
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Brockman, J.
1 / 1 shared
Collison, D.
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Teat, S. J.
1 / 5 shared
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Co-Authors (by relevance)

  • Nichol, Gary S.
  • Fazekas, Eszter
  • Etcheverry-Berrios, Alvaro
  • Piligkos, Stergios
  • Garden, Jennifer A.
  • Rajaraman, Gopalan
  • Dalgarno, Scott J.
  • Coletta, Marco
  • Jose, Reshma
  • Wilson, Lucinda R. B.
  • Sanz, Sergio
  • Parsons, Simon
  • Murrie, Mark
  • Moggach, Stephen A.
  • Probert, Michael R.
  • Kamenev, Konstantin V.
  • Meseguer, Carlos
  • Palacios, Maria A.
  • Drahos, Bohuslav
  • Colacio, Enrique
  • Mota, Antonio J.
  • Moreno, Jose M.
  • Navarrete, R.
  • Reinholdt, Anders
  • Mitcov, Dmitri
  • Wilhelm, Fabrice
  • Hassenkam, Tue
  • Gelardi, Rikke Munch
  • Thulstrup, Peter Waaben
  • Rogalev, Andrei
  • Wernsdorfer, Wolfgang
  • Konstantatos, Andreas
  • Pedersen, Anders H.
  • Vinum, Morten Gotthold
  • Sørensen, Mikkel Agerbæk
  • Ceccato, Marcel
  • Evangelisti, Marco
  • Uhrín, Dušan
  • Nielsen, Ulla Gro
  • Schnack, Jürgen
  • Fraser, Hector W. L.
  • Gro Nielsen, Ulla
  • Milios, Constantinos J.
  • Thomson, Andrew J.
  • Inglis, Ross
  • Bradley, Justin M.
  • Kamenev, Konstantin K.
  • Sanchez-Benitez, Javier
  • Moggach, S. A.
  • Lennie, A. R.
  • Warren, J. E.
  • Parois, P.
  • Parsons, S.
  • Murrie, M.
  • Prescimone, Alessandro
  • Warren, John E.
  • Lennie, Alistair R.
  • Parois, Pascal
  • Kortus, Jens
  • Loose, Claudia
  • Moggach, Stephen
  • Biagi, R.
  • Milios, C. J.
  • Pennino, U. Del
  • Corradini, V.
  • Jones, L. F.
  • Evangelisti, M.
  • Moro, F.
  • Renzi, V. De
  • Piligkos, S.
  • Wernsdorfer, W.
  • Sanudo, E. C.
  • Helliwell, M.
  • Christou, G.
  • Rajaraman, G.
  • Soler, M.
  • Slageren, J. Van
  • Kirchner, N.
  • Gudel, H. U.
  • Bircher, R.
  • Kortus, J.
  • Murugesu, M.
  • Raftery, J.
  • Teat, Simon J.
  • Sanudo, E. Carolina
  • Brockman, Jonathon
  • Christou, George
  • Murugesu, Muralee
  • Jones, Leigh F.
  • Collison, David
  • Raftery, Jim
  • Brockman, J.
  • Collison, D.
  • Teat, S. J.
OrganizationsLocationPeople

article

The effect of pressure on the crystal structure of [Gd(PhCOO)(3)(DMF)](n) to 3.7 GPa and the transition to a second phase at 5.0 GPa

  • Parsons, Simon
  • Warren, John E.
  • Lennie, Alistair R.
  • Parois, Pascal
  • Murrie, Mark
  • Moggach, Stephen A.
  • Brechin, Euan K.
Abstract

<p>The effect of pressure on the crystal structure of the coordination polymer [Gd(PhCOO)(3)(DMF)](n) has been studied to 5.0 GPa. At ambient pressure the structure is tetragonal (space group P4(2)/n) with the polymers extending along the c-direction of the unit cell; successive Gd atoms are alternately bridged by four benzoates and by two benzoates; the coordination spheres of the metal atoms are completed by DMF ligands. This results in two different Gd center dot center dot center dot Gd repeats, measuring 3.8953(3) and 5.3062(3) angstrom, respectively. The polymer chains interact with each other via dispersion interactions, including a number of CH center dot center dot center dot pi contacts to phenyl rings in which the H center dot center dot center dot ring-centroid distances are 3.19 to 3.28 angstrom. Up to 3.7 GPa the crystal remains in a compressed form of its ambient-pressure phase. The a-axis shortens by 7.7%, and the c-axis by 2.9%, the difference reflecting the greater ease of compression along the crystallographic directions mediated by weak intermolecular interactions. At ambient pressure the Gd-O distances span 2.290(2)-2.559(2) angstrom, with an average of 2.39(3) angstrom. At 3.7 GPa the corresponding parameters are 2.259(3) to 2.509(4) and 2.36(3) angstrom. The Gd center dot center dot center dot Gd distances shortened by 0.0467(4) and 0.1851(4) angstrom, and the CH center dot center dot center dot pi distances span the range 2.76-2.90 angstrom. During compression a number of H center dot center dot center dot H contacts develop, the shortest measuring 1.84 angstrom at 3.7 GPa. On increasing the pressure to 5.0 GPa a phase transition occurred in which the shortest H center dot center dot center dot H contact is relieved by conversion of an edge-to-edge phenyl-phenyl contact into a pi center dot center dot center dot pi stacking interaction. The new phase is also tetragonal, space group P (4) over bar 4, the inversion symmetry present in phase-I being lost in phase-II. The phase transition allows more efficient packing of ligands, and while the a-axis decreases in length the c-axis increases. This leads to Gd center dot center dot center dot Gd distances of 3.8373(4) and 5.3694(4) angstrom, the latter being longer than at ambient pressure. Gd-O distances at 5.0 GPa span the range 2.265(5) to 2.516(5) angstrom, with a mean of 2.36(2) angstrom.</p>

Topics
  • impedance spectroscopy
  • dispersion
  • polymer
  • phase
  • phase transition
  • space group