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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Skakle, Jan
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (11/11 displayed)
- 2021A pressure induced reversal to the 9R perovskite in Ba3MoNbO8.5citations
- 2011Synthesis of Bioceramic Compositions
- 2008Optimisation of the aqueous precipitation synthesis of silicatesubstituted hydroxyapatite
- 2008Optimisation of the aqueous precipitation synthesis of silicate-substituted hydroxyapatite
- 2007Comparison of Carbonate Hydroxyapatite with and without Sodium Co-Substitutioncitations
- 2007Synthesis of Novel High Silicate-Substituted Hydroxyapatite by Co-Substitution Mechanismscitations
- 2001Synthesis and characterisation of polymeric and oligomeric lead(II) carboxylatescitations
- 2001Structures of Mn(II) thiocyanate co-ordination polymers from flexible bipyridyl ligands
- 2001Synthesis of co-ordination networks from flexible bis-(4-pyridyl) ligands and cadmium saltscitations
- 2000Synthesis and crystal structure of [Mn(NCS)(2)L-2] (L=3,6-bis-(2-methylpyridyl)-1,2-pyridazine)
- 2000Synthesis and crystal structure of [Mn(NCS)2L2] (L = 3,6-bis-(2-methylpyridyl)-1,2-pyridazine)
Places of action
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article
Synthesis and characterisation of polymeric and oligomeric lead(II) carboxylates
Abstract
<p>The hydrothermal reactions of lead(II) acetate with carboxylic acids gave solids of composition [Pb(C4H4O4)] 1 (C4H4O4 = succinate); [Pb6O2(C14H9O3)(8)] 2 (C14H9O3 = benzoylbenzoate), [Pb(C8H4NO4)(2)(H2O)] 4 (C8H4NO4 = 2-nitrobenzoate) and [Pb(C8H3N2O6)(2)(H2O)] 5 (C8H3N2O6 = 3,5-dinitrobenzoate). The reaction of lead monoxide with trichloroacetic acid in hot wet toluene followed by filtration and cooling gave a solid of composition [Pb-3(C2Cl3O2)(6)(H2O)(3)] 3. The compounds were characterised by X-ray single crystal structure determinations. Compounds 1, 3, 4 and 5 are polymeric whereas 2 is monomeric. The lead co-ordination number ranges from 5 to 8. Compound 2 is a novel hexanuclear lead(II) distorted octahedron containing two bridging oxide ligands.</p>