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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Casas, Lluís
Universitat Autònoma de Barcelona
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2023Through the Looking Glass :citations
- 2019Breaking preconceptions: Thin section petrography for ceramic glaze microstructurescitations
- 2018Archaeometric study of African Keay 25.2 amphorae in Catalonia (Spain): A history of importation and imitationcitations
- 2016Establishing a new reference group of Keay 25.2 amphorae from Sidi Zahruni (Nabeul, Tunisia)citations
- 2015African terra sigillata from Henchir Es-Srira archaeological site, central Tunisia: Archaeological provenance and raw materials based on chemical analysiscitations
- 2014Provenance and reference groups of African Red Slip ware based on statistical analysis of chemical data and REEcitations
- 2011Structural and Mössbauer studies of aerosol FeCu nanoparticles in a wide composition rangecitations
- 2009Ordering and disordering processes in MA and MM intermetallic iron aluminide powderscitations
- 2004Ultraporous Single Phase Iron Oxide-Silica Nanostructured Aerogels from Ferrous Precursorscitations
- 2003Silica aerogel-iron oxide nanocomposites: Recoverable catalysts in conjugate additions and in the Biginelli reactioncitations
- 2003High-coercivity ultralight transparent magnetscitations
- 2001Silica aerogel-iron oxide nanocomposites: Structural and magnetic propertiescitations
Places of action
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article
Ultraporous Single Phase Iron Oxide-Silica Nanostructured Aerogels from Ferrous Precursors
Abstract
Monoliths of iron oxide-silica aerogel nanocomposites have been synthesized using a novel synthesis route which consists of impregnating silica wet gels with anhydrous iron(II) precursors followed by ethanol supercritical drying of the gels. The process yields aerogels exhibiting high porosity, large surface areas (∼900 m2/g), rather low densities (∼0.6 g/cm3), and a homogeneous distribution of single-phase maghemite, γ-Fe2O3, nanoparticles with average sizes in the 7-8 nm range. Remarkably, the γ-Fe2O3 nanoparticles are obtained in the as-dried state without the need of postannealing. The nanoparticles are mostly superparamagnetic at room temperature but become blocked in a ferrimagnetic state at lower temperatures.