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- 2016EPR spectroscopic characterization of a monomeric PtIII species produced via electrochemical oxidation of the anticancer compound trans-[PtII{(p-HC6F4)NCH2CH2NEt2}Cl(py)]citations
- 2011Synthesis and structural characterization of a TCNQ based organic semi-conducting material with a 2:5 stoichiometrycitations
- 2011Anion dependent redox changes in iron bis-terdentate nitroxide {NNO} chelatescitations
- 2011Controlled potential electrodeposition of a microcrystalline thin film of the charge transfer material tetrathiafulvalene-polyoxometalate of approximate composition (TTF)(5.3)(Bu4N)(0.7)[P2W18O62]center dot 3H(2)Ocitations
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article
Synthesis and structural characterization of a TCNQ based organic semi-conducting material with a 2:5 stoichiometry
Abstract
The tetrabutylammonium complex with a 2:5 stoichiometry, (n-Bu(4)N)(2)(TCNQ)(5), has been prepared and structurally characterized by X-ray crystallography. Diagnostic bands in the Raman spectrum and signature features in the electrochemistry confirm that the TCNQ moieties are partially charged in the solid state. EPR, magnetic susceptibility, and electrical conductivity measurements are all consistent with (n-Bu(4)N)(2)(TCNQ)(5) behaving as a quasi-one-dimensional organic semiconductor.