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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Canevali, Carmen
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Publications (6/6 displayed)
- 2023Studying stearic acid interaction with ZnO/SiO2 nanoparticles with tailored morphology and surface features: A benchmark for better designing efficient ZnO-based curing activatorscitations
- 2023Silica nanoparticles self-assembly process in polymer composites: Towards advanced materialscitations
- 2015Influence of doping elements on the formation rate of silicon nanowires by silver-assisted chemical etchingcitations
- 2003Nanocrystalline SnO2-Based Thin Films Obtained by Sol−Gel Route: A Morphological and Structural Investigationcitations
- 2003Nanocrystalline SnO2-Based Thin Films Obtained by Sol-Gel Route: A Morphological and Structural Investigationcitations
- 2002Optical properties of Ce3+-doped sol-gel silicate glassescitations
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article
Nanocrystalline SnO2-Based Thin Films Obtained by Sol−Gel Route: A Morphological and Structural Investigation
Abstract
The thermal evolution of sol−gel SnO2-based thin films was explored by investigating their structural and morphological features. Nanostructured SnO2 and Pt-doped SnO2 layers were obtained using tetra(tert-butoxy)tin(IV) and Pt(II) acetlylacetonate as precursors. Films were prepared by spin coating from ethanol solutions with different viscosity. After drying at room temperature, they were annealed in air at 673 and 973 K. The surface morphology was analyzed by scanning electron microscopy, atomic force microscopy, and scanning near-field optical microscopy. The structural characterization was performed by means of glancing incidence X-ray diffraction and microdiffraction. Both drying at room temperature and thermal treatment at 673 K resulted in the formation of holes on the surface and inside the films. Their distribution and average dimension were found to depend mainly on the viscosity of the sol precursor, and on the presence of Pt in the films. After annealing at 973 K, surface segregation of PtOx p...