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Pääkkönen, Timo
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Publications (5/5 displayed)
- 2022Effect of Moisture on Polymer Deconstruction in HCl Gas Hydrolysis of Woodcitations
- 2021Visualizing Degradation of Cellulose Nanofibers by Acid Hydrolysiscitations
- 2019Sustainable High Yield Route to Cellulose Nanocrystals from Bacterial Cellulosecitations
- 2019Sustainable High Yield Route to Cellulose Nanocrystals from Bacterial Cellulosecitations
- 2016Effect of xylan in hardwood pulp on the reaction rate of TEMPO-mediated oxidation and the rheology of the final nanofibrillated cellulose gelcitations
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article
Sustainable High Yield Route to Cellulose Nanocrystals from Bacterial Cellulose
Abstract
HCl gas hydrolysis of a bacterial cellulose (BC) aerogel followed by 2,2,6,6-tetramethylpiperidine-1-oxyl radical-mediated oxidation was used to produce hydrolyzed BC with carboxylate groups, which subsequently disintegrated into a stable dispersion of cellulose nanocrystals (CNCs). The degree of polymerization was successfully reduced from 2160 to 220 with a CNC yield of >80%. ; Peer reviewed