People | Locations | Statistics |
---|---|---|
Naji, M. |
| |
Motta, Antonella |
| |
Aletan, Dirar |
| |
Mohamed, Tarek |
| |
Ertürk, Emre |
| |
Taccardi, Nicola |
| |
Kononenko, Denys |
| |
Petrov, R. H. | Madrid |
|
Alshaaer, Mazen | Brussels |
|
Bih, L. |
| |
Casati, R. |
| |
Muller, Hermance |
| |
Kočí, Jan | Prague |
|
Šuljagić, Marija |
| |
Kalteremidou, Kalliopi-Artemi | Brussels |
|
Azam, Siraj |
| |
Ospanova, Alyiya |
| |
Blanpain, Bart |
| |
Ali, M. A. |
| |
Popa, V. |
| |
Rančić, M. |
| |
Ollier, Nadège |
| |
Azevedo, Nuno Monteiro |
| |
Landes, Michael |
| |
Rignanese, Gian-Marco |
|
Vitorica-Yrezabal, Inigo J.
Universidad de Granada
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2024Two‐ and Three‐Spin Hybrid Inorganic‐Organic [2]Rotaxanes Containing Metallated Salen Groups
- 2022Adsorption of sulphur dioxide in Cu(II)-carboxylate framework materials: the role of ligand functionalisation and open metal sites
- 2022Investigating the effect of steric hindrance within CdS single-source precursors on the material properties of AACVD and spin coat-deposited CdS thin filmscitations
- 2021Structural investigations of α-MnS nanocrystals and thin films synthesised from manganese(II) xanthates by hot injection, solvent-less thermolysis and doctor blade routes.citations
- 2020Single-Step Enantioselective Synthesis of Mechanically Planar Chiral [2]Rotaxanes Using a Chiral Leaving Group Strategycitations
- 2020Single-Step Enantioselective Synthesis of Mechanically Planar Chiral [2]Rotaxanes Using a Chiral Leaving Group Strategycitations
- 2019Synthesis of Iron Sulfide Thin Films and Powders from New Xanthate Precursorscitations
- 2019Chemical vapor deposition of tin sulfide from diorganotin(IV) dixanthatescitations
- 2019Accessing γ-Ga2S3 by solventless thermolysis of gallium xanthates: A low temperature limit for crystalline products?citations
- 2018Synthesis of Nanostructured Powders and Thin Films of Iron Sulfide from Molecular Precursorscitations
- 2018The synthesis of a monodisperse quaternary ferrite (FeCoCrO4) from the hot injection thermolysis of the single source precursor [CrCoFeO(O2C: TBu)6(HO2CtBu)3]citations
- 2017The synthesis of group 10 and 11 metal complexes of 3,6,9-trithia- 1-(2,6)-pyridinacyclodecaphane and their use in A3-coupling reactionscitations
- 2017Arene guest selectivity and pore flexibility in a metal–organic framework with semi-fluorinated channel wallscitations
- 2017Portraying entanglement between molecular qubits with four-dimensional inelastic neutron scatteringcitations
Places of action
Organizations | Location | People |
---|
article
Structural investigations of α-MnS nanocrystals and thin films synthesised from manganese(II) xanthates by hot injection, solvent-less thermolysis and doctor blade routes.
Abstract
Manganese (II) xanthate complexes of the form [Mn(S2COR)2(TMEDA)], where TMEDA = tetramethylethylenediamine and R = methyl (1), ethyl (2), n-propyl (3), n-butyl (4), n-pentyl (5), n-hexyl (6) and n-octyl (7), have been synthesised and structures elucidated using single crystal X-ray diffraction. Complexes 1 to 7 were used as molecular precursors to synthesise manganese sulfide (MnS). Olelyamine (OLA) capped nanocrystals have been produced via hot injection, whilst the doctor blading followed by thermolysis yielded thick films. Free-standing polycrystalline powders of MnS are produced by direct thermolysis of precursor powders. All thermolysis techniques produced cubic MnS as confirmed by powder X-ray diffraction, scanning electron microscopy (SEM), energy dispersive X-ray (EDX) spectroscopy and Raman spectroscopy. Magnetic measurements reveal that the α-MnS nanocrystals exhibit ferromagnetic behaviour with a large coercive field strength (e.g., 0.723 kOe for 6.8 nm nanocrystals).