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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Fernando, Gerard
University of Birmingham
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (22/22 displayed)
- 2023Effects of NaOH treatment and NaOH treatment conditions on the mechanical properties of coir fibres for use in composites manufacturecitations
- 2023Simultaneous multi-measurand analyses of cross-linking reactions within a differential scanning calorimeter using optical fibre sensorscitations
- 2023Single-Solvent Fractionation and Electro-Spinning Neat Softwood Kraft Lignincitations
- 2022Monitoring Cross-Linking, the Evolution of Refractive Index and the Glass Transition Temperature of an Epoxy Resin Using an Optical Fiber Sensorcitations
- 2021Vertically-aligned short E-glass fibre core sandwich composite: Production and evaluationcitations
- 2021Improved procedure for electro-spinning and carbonisation of neat solvent-fractionated softwood Kraft lignincitations
- 2016Monitoring pre-stressed composites using optical fibre sensorscitations
- 2016In-situ monitoring of cross-linking reactions using E-glass fibres and evanescent wave spectroscopycitations
- 2014Multi-point monitoring of cross-linking reactionscitations
- 2012Lateral spreading of a fiber bundle via mechanical meanscitations
- 2011Synthesis of Ag/AgCl-mesoporous silica nanocomposites using a simple aqueous solution-based chemical method and a study of their antibacterial activity on E. colicitations
- 2010Evaluation of Embedded Optical Fiber Composites: EFPI Sensor Response to Sensors in Fatigue Loadingcitations
- 2009In-situ damage detection using self-sensing compositescitations
- 2009Evaluation of embedded optical fiber sensors in composites: EFPI sensor fabrication and quasi-static evaluationcitations
- 2009A comparison of cure monitoring techniquescitations
- 2008A novel fibre optic acoustic emission sensorcitations
- 2008Chemical process monitoring and the detection of moisture ingress in composites - art. no. 69330R
- 2007Smart materials and systems
- 2007Fabrication of intrinsic fibre Fabry–Perot sensors in silica fibres using hydrofluoric acid etchingcitations
- 2006Process monitoring of fibre reinforced composites using optical fibre sensorscitations
- 2006Investigation of reversible photo-mechanical properties of azobenzene-based polymer films by nano-indentationcitations
- 2002A Method To Measure The Interfacial Shear Stress For Optical Fibres Embedded In Fibre Reinforced Composites
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article
Single-Solvent Fractionation and Electro-Spinning Neat Softwood Kraft Lignin
Abstract
This paper reports on the production of electro-spun nanofibers from softwood Kraft lignin without the need for polymer blending and/or chemical modification. Commercially available softwood Kraft lignin was fractionated using acetone. The acetone-soluble lignin (AcSL) had an ash content of 0.06 wt %, a weight average molecular weight of 4250 g·mol–1 along with the polydispersity index of 1.73. The corresponding values for as-received lignin (ARL) were 1.20 wt %, 6000 g·mol–1, and 2.22, respectively. The AcS was dissolved in a binary solvent consisting of acetone, and dimethyl sulfoxide (2:1, v/v) was selected for dissolving the AcSL. Conventional and custom-designed grounded electrode configurations were used to produce electro-spun neat lignin fibers that were randomly oriented or highly aligned, respectively. The diameter of the electro-spun fibers ranged from 1.12 to 1.46 μm. After vacuum drying at 140 °C for 6 h to remove the solvents and oxidation at 250 °C, the fibers were carbonized at 1000, 1200, and 1500 °C for 1 h. The carbonized fibers were unfused and void-free with an average diameter of 500 nm. Raman spectroscopy, scanning electron microscopy, and image analysis were used to characterize the carbonized fibers.