693.932 PEOPLE
| People | Locations | Statistics |
|---|---|---|
| Naji, M. |
| |
| Motta, Antonella |
| |
| Aletan, Dirar |
| |
| Mohamed, Tarek |
| |
| Ertürk, Emre |
| |
| Taccardi, Nicola |
| |
| Kononenko, Denys |
| |
| Petrov, R. H. | Madrid |
|
| Alshaaer, Mazen | Brussels |
|
| Bih, L. |
| |
| Casati, R. |
| |
| Muller, Hermance |
| |
| Kočí, Jan | Prague |
|
| Šuljagić, Marija |
| |
| Kalteremidou, Kalliopi-Artemi | Brussels |
|
| Azam, Siraj |
| |
| Ospanova, Alyiya |
| |
| Blanpain, Bart |
| |
| Ali, M. A. |
| |
| Popa, V. |
| |
| Rančić, M. |
| |
| Ollier, Nadège |
| |
| Azevedo, Nuno Monteiro |
| |
| Landes, Michael |
| |
| Rignanese, Gian-Marco |
|
Mugnaioli, Enrico
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (23/23 displayed)
- 2022Halide perovskites as disposable epitaxial templates for the phase-selective synthesis of lead sulfochloride nanocrystalscitations
- 2021Titania-decorated hybrid nano-architectures and their preliminary assessment in catalytic applications
- 2020Structural study of decrespignyite-(Y), a complex yttrium rare earth copper carbonate chloride, by three-dimensional electron and synchrotron powder diffraction
- 2020Nanocrystals of Lead Chalcohalides:A Series of Kinetically Trapped Metastable Nanostructurescitations
- 2020Nanocrystals of Lead Chalcohalidescitations
- 2020Cs 3 Cu 4 In 2 Cl 13 Nanocrystals:A Perovskite-Related Structure with Inorganic Clusters at A Sitescitations
- 2020Cs3Cu4In2Cl13 Nanocrystalscitations
- 20193D Electron Diffraction: The Nanocrystallography Revolutioncitations
- 2018Crystal Structures of Two Important Pharmaceuticals Solved by 3D Precession Electron Diffraction Tomographycitations
- 2018Ab initio structure determination of Cu2- xTe plasmonic nanocrystals by precession-assisted electron diffraction tomography and HAADF-STEM imagingcitations
- 2018Ab Initio Structure Determination of Cu2- xTe Plasmonic Nanocrystals by Precession-Assisted Electron Diffraction Tomography and HAADF-STEM Imagingcitations
- 2017Mineralogical, crystallographic and redox features of the earliest stages of fluid alteration in CM chondritescitations
- 2017The structure of denisovite, a fibrous nanocrystalline polytypic disordered 'very complex' silicate, studied by a synergistic multi-disciplinary approach employing methods of electron crystallography and X-ray powder diffractioncitations
- 2017The structure of denisovite, a fibrous nanocrystalline polytypic disordered 'very complex' silicate, studied by a synergistic multi-disciplinary approach employing methods of electron crystallography and X-ray powder diffractioncitations
- 2016Hierachical Ni@Fe2O3 superparticles through epitaxial growth of gamma-Fe2O3 nanorods on in situ formed Ni nanoplatescitations
- 2015Electron diffraction tomography for the characterization of sub-micrometric minerals: application to metamict phases
- 2015Structural insights into<i>M</i><sub>2</sub>O–Al<sub>2</sub>O<sub>3</sub>–WO<sub>3</sub>(<i>M</i>= Na, K) system by electron diffraction tomographycitations
- 2015Structural insights into M2O–Al2O3–WO3 (M = Na, K) system by electron diffraction tomographycitations
- 2015Single nano crystal analysis using automated electron diffraction tomographycitations
- 2014Rational assembly and dual functionalization of Au@MnO heteroparticles on TiO2 nanowirescitations
- 2014Atomic structure solution of the complex quasicrystal approximant Al77Rh15Ru8 from electron diffraction datacitations
- 2013A multi-technique characterisation of cronstedtite synthetized by iron-clay interaction in a step by step cooling procedurecitations
- 2009Electron diffraction, X-ray powder diffraction and pair-distribution-function analyses to determine the crystal structures of Pigment Yellow 213, C<sub>23</sub>H<sub>21</sub>N<sub>5</sub>O<sub>9</sub>citations
Places of action
| Organizations | Location | People |
|---|
article
Crystal Structures of Two Important Pharmaceuticals Solved by 3D Precession Electron Diffraction Tomography
Abstract
The crystal structures of two important marketed pharmaceuticals, namely, ramelteon (RAM) and tolvaptan (TOL), were determined for the first time using 3D precession electron diffraction tomography (PEDT) on 500 nm-sized crystals. The results were compared with the same structures determined by single-crystal X-ray diffraction on subsequently grown 50−200 μm single crystals, indicating a good match of molecular conformation, crystal packing, and unit cell parameters.<br/>The X-ray crystal structures were used to validate the developed workflow of data acquisition and structure solution with electron diffraction. This study highlights that 3D PEDT alone is able to provide accurate crystal structures from pharmaceutical nanocrystals that will suffice for most practical applications when no larger crystals can be grown.