| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Kasama, Takeshi
Technical University of Denmark
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (29/29 displayed)
- 2019Electron holographycitations
- 2018Optimal microstructural design for high thermal stability of pure FCC metals based on studying effect of twin boundaries character and network of grain boundariescitations
- 2018Optimal microstructural design for high thermal stability of pure FCC metals based on studying effect of twin boundaries character and network of grain boundariescitations
- 2018Probing the chemistry of adhesion between a 316L substrate and spin-on-glass coatingcitations
- 2018Mechanisms of Se(IV) Co-precipitation with Ferrihydrite at Acidic and Alkaline Conditions and Its Behavior during Agingcitations
- 2018Magnetically activated microcapsules as controlled release carriers for a liquid PDMS cross-linkercitations
- 2018Transformation of iron containing constituent intermetallic particles during hydrothermal treatment
- 2017Mechanical properties of multilayer Ni-Fe and Ni-Fe-Al2O3 nanocomposite coatingcitations
- 2017Mechanical properties of multilayer Ni-Fe and Ni-Fe-Al 2 O 3 nanocomposite coatingcitations
- 2016Origin of Spontaneous Core-Shell AIGaAs Nanowires Grown by Molecular Beam Epitaxycitations
- 2015Influence of aging products on tensile deformation behavior of Al-0.62 mass%Mg-0.32 mass%Si alloycitations
- 2014Interferometric methods for mapping static electric and magnetic fieldscitations
- 2014Transmission electron microscopy of unstained hybrid Au nanoparticles capped with PPAA (plasma-poly-allylamine):Structure and electron irradiation effectscitations
- 2014Transmission electron microscopy of unstained hybrid Au nanoparticles capped with PPAA (plasma-poly-allylamine)citations
- 2014Off-axis electron holography of ferromagnetic multilayer nanowirescitations
- 20143D visualization of TiO2 nanocrystals in mesoporous nanocomposite using energy filtered transmission electron microscopy tomographycitations
- 2014Towards quantitative off-axis electron holographic mapping of the electric field around the tip of a sharp biased metallic needlecitations
- 2014Magnetic characterization of synthetic titanomagnetites: quantifying the recording fidelity of ideal synthetic analogscitations
- 2013Ferrimagnetic/ferroelastic domain interactions in magnetite below the Verwey transition. Part I: electron holography and Lorentz microscopycitations
- 2013Oxidation of Dodecanoate Intercalated Iron(II)–Iron(III) Layered Double Hydroxide to Form 2D Iron(III) (Hydr)oxide Layerscitations
- 2013Ferrimagnetic/ferroelastic domain interactions in magnetite below the Verwey transition: Part II. Micromagnetic and image simulationscitations
- 2011Formation process and superparamagnetic properties of (Mn,Ga)As nanocrystals in GaAs fabricated by annealing of (Ga,Mn)As layers with low Mn content
- 2011Formation process and superparamagnetic properties of (Mn,Ga)As nanocrystals in GaAs fabricated by annealing of (Ga,Mn)As layers with low Mn contentcitations
- 2011Spin reorientation in α-Fe2O3 nanoparticles induced by interparticle exchange interactions in alpha-Fe2O3/NiO nanocompositescitations
- 2011Voids and Mn-rich inclusions in a (Ga,Mn)As ferromagnetic semiconductor investigated by transmission electron microscopycitations
- 2010Direct observation of ferrimagnetic/ferroelastic domain interactions in magnetite below the Verwey transitioncitations
- 2010Interpretation of electron beam induced charging of oxide layers in a transistor studied using electron holographycitations
- 2010Nonadiabatic Spin Torque Investigated Using Thermally Activated Magnetic Domain Wall Dynamicscitations
- 2006Periodic inclusion of room-temperature-ferromagnetic metal phosphide nanoparticles in carbon nanotubescitations
Places of action
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article
Probing the chemistry of adhesion between a 316L substrate and spin-on-glass coating
Abstract
Hydrogen silsesquioxane ([HSiO<sub>3/2</sub>]<sub>n</sub>) based "spin-on-glass" has been deposited on 316L substrate and cured in Ar/H<sub>2</sub> gas atmosphere at 600 ºC to form a continuous surface coating with sub-micrometer thickness. The coating functionality depends primarily on the adhesion to the substrate, which is largely affected by the chemical interaction at the interface between the coating and the substrate. We have investigated this interface by transmission electron microscopy and electron energy loss spectroscopy. The analysis identified a 5-10 nm thick interaction zone containing signals from O, Si, Cr and Fe. Analysis of the energy loss near edge structure of the present elements identified predominantly signal from [SiO<sub>4</sub>]<sup>4-</sup> units together with Fe<sup>2+</sup>, Cr<sup>2+</sup> and traces of Cr<sup>3+</sup>. High-resolution transmission electron microscopy images of the interface region confirm a crystalline Fe<sub>2</sub>SiO<sub>4</sub> interfacial region. In agreement with computational thermodynamics, it is proposed that the spin-on-glass forms a chemically bonded silicate-rich interaction zone with the substrate. It was further suggested that this zone is composed of a corundum-type oxide at the substrate surface, followed by an olivine-structure intermediate phase and a spinel-type oxide in the outer regions of the interfacial zone.