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Curtis, Anna C.
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article
Purification of Oleylamine for Materials Synthesis and Spectroscopic Diagnostics for trans Isomers
Abstract
<p>Oleylamine is widely used in nanomaterial and metal-halide perovskite synthesis. Impurities in commercially available oleylamine reagents are identified, purification procedures are explained, beneficial effects on lead chloride/oleylamine mixtures are documented, and impacts on materials synthesis are discussed. Suspensions of 0.12 mole fraction PbCl<sub>2</sub>, PbBr<sub>2</sub>, and PbI<sub>2</sub>in purified, dried, and filtered oleylamine were found to form clear solutions upon heating to 100 °C. The infrared, Raman, and NMR spectra of oleylamine and a common trans impurity present in literature reference IR spectra are presented.</p>