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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Zou, Xiaodong
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (15/15 displayed)
- 2023Accurate structure models and absolute configuration determination using dynamical effects in continuous-rotation 3D electron diffraction datacitations
- 2023Accurate structure models and absolute configuration determination using dynamical effects in continuous-rotation 3D electron diffraction data
- 2022Metal-hydrogen-pi-bonded organic frameworkscitations
- 2021Probing Molecular Motions in Metal-Organic Frameworks by Three-Dimensional Electron Diffractioncitations
- 2021A Tunable Multivariate Metal–Organic Framework as a Platform for Designing Photocatalystscitations
- 2019Solving a new R2lox protein structure by microcrystal electron diffractioncitations
- 2019Luminescence properties of a family of lanthanide metal-organic frameworkscitations
- 2019A metal-organic framework for efficient water-based ultra-low-temperature-driven coolingcitations
- 2018Multidimensional Disorder in Zeolite IM-18 Revealed by Combining Transmission Electron Microscopy and X-ray Powder Diffraction Analysescitations
- 2018Chitosan enhances gene delivery of oligonucleotide complexes with magnetic nanoparticles–cell-penetrating peptide ...
- 2017Disordered zeolite solved by combining electron diffraction, HRTEM and XRPD
- 2014Correlated defect nanoregions in a metal–organic frameworkcitations
- 2013Sustainable Catalysis : Rational Pd Loading on MIL-101Cr-NH2 for More Efficient and Recyclable Suzuki-Miyaura Reactionscitations
- 2013Sustainable Catalysis: Rational Pd Loading on $MIL-101Cr-NH_{2}$ for More Efficient and Recyclable Suzuki-Miyaura Reactionscitations
- 2012Structure and catalytic properties of the most complex intergrown zeolite ITQ-39 determined by electron crystallographycitations
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article
Multidimensional Disorder in Zeolite IM-18 Revealed by Combining Transmission Electron Microscopy and X-ray Powder Diffraction Analyses
Abstract
International audience ; A new medium-pore germanosilicate, denoted IM-18, with a three-dimensional 8 × 8 × 10-ring channel system, has been prepared hydrothermally using 4-dimethylaminopyridine as an organic structure-directing agent (OSDA). Due to the presence of stacking disorder, the structure elucidation of IM-18 was challenging, and a combination of different techniques, including electron diffraction, high-resolution transmission electron microscopy (HRTEM), and Rietveld refinement using synchrotron powder diffraction data, was necessary to elucidate the details of the structure and to understand the nature of the disorder. Rotation electron diffraction data were used to determine the average structure of IM-18, HRTEM images to characterize the stacking disorder, and Rietveld refinement to locate the Ge in the framework and the OSDA occluded in the channels