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Grabias, A.
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article
Phase transformations in the Fe(Co,Ni) ZrB alloys induced by ball milling
Abstract
Phase transformations in the FeZrB-based powders induced by high- and low-energy ball milling are investigated by X-ray diffraction and transmission Mössbauer spectroscopy. The structural and magnetic properties of the processed powders are studied as a function of milling time. The influence of Co and Ni additions on the phase transformations is also investigated. X-ray diffraction measurements of the high-energy ball milled powders indicate the formation of the b.c.c. Fe solid solution. Mössbauer results, however, reveal more complex structure of the milled powders, in particular, the formation of an FeZr amorphous phase at the early stages of milling as well as formation of Fe–B phases. The low-energy ball milling is found to be poorly effective in the alloying of the elemental FeZrB-based powders.