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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Liu, Yanwen
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (22/22 displayed)
- 2024Multi-Analytical Study of Damage to Marine Ballast Tank Coatings After Cyclic Corrosion Testing
- 2024High resolution analytical microscopy of damage progression within a polyester powder coating after cyclic corrosion testing
- 2021Local oxidation of the buried epoxy-amine/iron oxide interphasecitations
- 2021Local Oxidation of the Buried Epoxy-Amine / Iron Oxide Interphase
- 2020Examining the early stages of thermal oxidative degradation in epoxy-amine resinscitations
- 2019Leaching from coatings pigmented with strontium aluminium polyphosphate inhibitor pigment- evidence for a cluster-percolation modelcitations
- 2019How pigment volume concentration (PVC) and particle connectivity affect leaching of corrosion inhibitive species from coatingscitations
- 2018Multi-Modal Plasma Focused Ion Beam Serial Section Tomography of an Organic Paint Coatingcitations
- 2017Molecularly Controlled Epoxy Network Nanostructurescitations
- 2017Time-lapse lab-based X-ray nano-CT study of corrosion damagecitations
- 2017An organic coating pigmented with strontium aluminium polyphosphate for corrosion protection of zinc alloy coated steelcitations
- 2017An organic coating pigmented with strontium aluminium polyphosphate for corrosion protection of zinc alloy coated steelcitations
- 2017Influence of Volume Concentration of Active Inhibitor on Microstructure and Leaching Behaviour of a Model Primercitations
- 2016Lithium salts as leachable corrosion inhibitors and potential replacement for hexavalent chromium in organic coatings for the protection of aluminum alloyscitations
- 2016Corrosion inhibition of pure aluminium and AA2014-T6 alloy by strontium chromate at low concentrationcitations
- 2016An investigation of the corrosion inhibitive layers generated from lithium oxalatecontaining organic coating on AA2024-T3 aluminium alloycitations
- 2015The corrosion protection of AA2024-T3 aluminium alloy by leaching of lithium-containing salts from organic coatingscitations
- 2015The corrosion protection of AA2024-T3 aluminium alloy by leaching of lithium-containing salts from organic coatingscitations
- 2015Protective Film Formation on AA2024-T3 Aluminum Alloy by Leaching of Lithium Carbonate from an Organic Coating
- 2010Corrosion behaviour of mechanically polished AA7075-T6 aluminium alloycitations
- 2006Morphology, composition and structure of anodic films on binary Al-Cu alloyscitations
- 2002Imaging XPS investigation of the lateral distribution of copper inclusions at the abraded surface of 2024T3 aluminium alloy and adsorption of decyl phosphonic acidcitations
Places of action
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article
Multi-Modal Plasma Focused Ion Beam Serial Section Tomography of an Organic Paint Coating
Abstract
Pigment distributions have a critical role in the corrosion protection properties of organic paint coatings, but they are difficult to image in 3D over statistically significant volumes and at sufficiently high spatial resolutions required for detailed analysis. Here we report, for the first time, large volume analytical serial sectioning tomography of an organic composite coating using a xenon Plasma Focused Ion Beam (PFIB) combined with secondary electron imaging, energy dispersive X-ray (EDX) spectrum imaging (SI) and electron backscattered diffraction (EBSD). Together these techniques provide a comprehensive quantitative description of the physical orientation and distribution of the pigments within a model marine ballast tank coating, as well as their crystallographic and elemental characterisation. Polymers and organic materials are challenging because of their propensity for ion beam damage and possible beam heating effects. Our novel, optimised block preparation technique permits automated data acquisition with minimal operator intervention, and can have significant applications for the structural and chemical characterisation of a wide range of organic materials.Our results revealed that the paint contained 7.5 vol% aluminium flakes and 25 vol% quartz particles. The aluminium flakes were oriented parallel to the substrate surface, which is beneficial in terms of the corrosion protection capability of the coating.