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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Daly, Michael
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (12/12 displayed)
- 2024Mechanical and crystallization properties of hot runner injection molded virgin and recycled polypropylenecitations
- 2021Acute and longer-term psychological distress associated with testing positive for COVID-19: longitudinal evidence from a population-based study of US adultscitations
- 2017A multi-scale correlative investigation of ductile fracturecitations
- 2017Degradation of metallic materials studied by correlative tomographycitations
- 2016Synthesis and characterization of high density polyethylene/peat ash compositescitations
- 2016Chemical surface modification of calcium carbonate particles with stearic acid using different treating methodscitations
- 2016Characteristics of the treated calcium carbonate particles with stearic acid using different treating methods. ; Chemical surface modification of calcium carbonate particles with stearic acid using different treating methods
- 2015Large volume serial section tomography by Xe Plasma FIB dual beam microscopycitations
- 2015Large volume serial section tomography by Xe Plasma FIB dual beam microscopycitations
- 2013Advanced assessment of the ductile fracture mechanism in A508 class 3 reactor pressure vessel steel using laboratory X-ray tomographycitations
- 2013Advanced assessment of ductile tearing in nuclear reactor pressure vessel steel using x-ray tomography
- 2012Advanced assessment of the integrity of ductile components
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article
Large volume serial section tomography by Xe Plasma FIB dual beam microscopy
Abstract
Ga+ Focused Ion Beam-Scanning Electron Microscopes (FIB-SEM) have revolutionised the level of microstructural information that can be recovered in 3D by block face serial section tomography (SST), as well as enabling the site-specific removal of smaller regions for subsequent transmission electron microscope (TEM) examination. However, Ga+ FIB material removal rates limit the volumes and depths that can be probed to dimensions in the tens of microns range. Emerging Xe+ Plasma Focused Ion Beam-Scanning Electron Microscope (PFIB-SEM) systems promise faster removal rates. Here we examine the potential of the method for large volume serial section tomography as applied to bainitic steel and WC–Co hard metals. Our studies demonstrate that with careful control of milling parameters precise automated serial sectioning can be achieved with low levels of milling artefacts at removal rates some 60× faster. Volumes that are hundreds of microns in dimension have been collected using fully automated SST routines in feasible timescales (