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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Favache, Audrey
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Publications (7/7 displayed)
- 2023Effect of the nanopores in the Al-Cu intermetallic phase on nanoindentation instabilities at the Al/Cu interface of a magnetic pulse impact weldcitations
- 2019High-throughput Experimental Design of High-Entropy Alloys
- 2018Effect of hydriding induced defects on the small-scale plasticity mechanisms in nanocrystalline palladium thin filmscitations
- 2017Mechanical behavior of ultrathin sputter deposited porous amorphous Al2O3 filmscitations
- 2015Fracture mechanics based analysis of the scratch resistance of thin brittle coatings on a soft interlayercitations
- 2014Fracture toughness measurement of ultra-thin hard films deposited on a polymercitations
- 2014Analysis of the variation in nanohardness of pearlitic steel: Influence of the interplay between ferrite crystal orientation and cementite morphologycitations
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article
Fracture toughness measurement of ultra-thin hard films deposited on a polymer
Abstract
The fracture toughness of 100 nm-thick chromium nitride films deposited on a soft interlayer is evaluated using two different test methods. Both methods take advantage of the enhanced crack driving force resulting fromthe large elastic stiffness mismatch between the film and the polymer interlayer. The first method is based on the presence of channel cracks developing during the deposition as a result of large internal stress. The second method relies on nanoindentation induced cracking. The presence of a soft interlayer is shown to be essential to promote cracking otherwise impossible on a hard substrate, hence to determine the fracture toughness of very thin films. The assumptions underlying the two methods are very different, which allows critical cross comparison and assessment. A fracture toughness value between 1.5 and 2MPa·m1/2 is obtained.