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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Farjas, Jordi
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (18/18 displayed)
- 2022Chemical and Microstructural Nanoscale Homogeneity in Superconducting YBa2Cu3O7-x Films Derived from Metal-Propionate Fluorine-free Solutionscitations
- 2021High Performance of Superconducting YBa2Cu3O7 Thick Films Prepared by Single-Deposition Inkjet Printing
- 2020Ultrafast transient liquid assisted growth of high current density superconducting films
- 2020Ultrafast transient liquid assisted growth of high current density superconducting films
- 2020Relevance of the Formation of Intermediate Non-Equilibrium Phases in YBa2Cu3O7-x Film Growth by Transient Liquid-Assisted Growth
- 2020Elucidation of the decomposition reactions of low-fluorine YBa2Cu3O7-x precursors during film pyrolysis
- 2019Thermal decomposition of CuProp2: In-situ analysis of film and powder pyrolysiscitations
- 2018Epitaxial superconducting GdBa2Cu3O7−δ /Gd2O3 nanocomposite thin films from advanced low-fluorine solutionscitations
- 2015Thermal analysis of metal organic precursors for functional oxide preparation: Thin films versus powderscitations
- 2015The effect of volatiles on the measurement of the reaction heat by differential scanning calorimetrycitations
- 2013Thermal decomposition of barium trifluoroacetate thin filmscitations
- 2013Thermoanalytical study of the decomposition of yttrium trifluoroacetate thin filmscitations
- 2012Synthesis of nanocrystalline ceria thin films by low-temperature thermal decomposition of Ce-propionatecitations
- 2011Thermoanalytical study of the formation mechanism of yttria from yttrium acetatecitations
- 2009Characterization of amorphous and nanostructured Si films by differential scanning calorimetrycitations
- 2007Numerical model of solid phase transformations governed by nucleation and growth: Microstructure development during isothermal crystallizationcitations
- 2002Calorimetry of hydrogen desorption from a-Si nanoparticlescitations
- 2001Enhancement of oxidation rate of a-Si nanoparticles during dehydrogenationcitations
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article
Characterization of amorphous and nanostructured Si films by differential scanning calorimetry
Abstract
Over the last 5 years, we have successfully applied differential scanning calorimetry (DSC) to study silicon thin films. The aim of this paper is to review our main results to give an overview of the possibilities offered by this technique, which is widely used to characterize solid state transformations. We will address some classical subjects related to the structure of pure and hydrogenated a-Si, such as the strength of the Si-H bond, hydrogen diffusion and the contribution of structural defects and strained bonds to the enthalpy of structural relaxation and crystallization. Special attention will be paid to the crystallization kinetics of films with structures ranging from pure amorphous to highly crystalline. Despite previous expectations, in films deposited at low temperature, the presence of nanocrystals embedded in the amorphous phase does not promote crystallization. In fact, the crystallization temperature is much higher than expected from a simple solid state epitaxy mechanism, which indicates low coupling between the amorphous and crystalline phases. © 2009 Elsevier B.V. All rights reserved.