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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Terzopoulou, Zoi
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (16/16 displayed)
- 2024Valorization of Tomato Agricultural Waste for 3D-Printed Polymer Composites Based on Poly(lactic acid)citations
- 2023Poly(Lactic Acid) Composites with Lignin and Nanolignin Synthesized by In Situ Reactive Processing
- 2023Poly(Lactic Acid) Composites with Lignin and Nanolignin Synthesized by In Situ Reactive Processingcitations
- 2022Revisiting Non-Conventional Crystallinity-Induced Effects on Molecular Mobility in Sustainable Diblock Copolymers of Poly(propylene adipate) and Polylactidecitations
- 2021Synthesis, Properties, and Enzymatic Hydrolysis of Poly(lactic acid)- co -Poly(propylene adipate) Block Copolymers Prepared by Reactive Extrusion
- 2021Comparative study of crystallization, semicrystalline morphology, and molecular mobility in nanocomposites based on polylactide and various inclusions at low filler loadingscitations
- 2021Synthesis and Characterization of Unsaturated Succinic Acid Biobased Polyester Resinscitations
- 2021Preparation of green montmorillonite/carbon nanotubes hybrid by lyophilization procedure for poly(lactic acid) nanocomposite
- 2021Cold Crystallization Kinetics and Thermal Degradation of PLA Composites with Metal Oxide Nanofillerscitations
- 2021Synthesis, Properties, and Enzymatic Hydrolysis of Poly(lactic acid)-co-Poly(propylene adipate) Block Copolymers Prepared by Reactive Extrusioncitations
- 2019Sustainable thermoplastics from renewable resources:Thermal behavior of poly(1,4-cyclohexane dimethylene 2,5-furandicarboxylate)citations
- 2019Sustainable thermoplastics from renewable resourcescitations
- 2018Effect of surface functionalization of halloysite nanotubes on synthesis and thermal properties of poly(ε-caprolactone)citations
- 2018Synthesis and characterization of in-situ-prepared nanocomposites based on poly(propylene 2,5-furan dicarboxylate) and aluminosilicate clayscitations
- 2017Effect of MWCNTs and their modification on crystallization and thermal degradation of poly(butylene naphthalate)citations
- 2014Effect of nanofiller's size and shape on the solid state microstructure and thermal properties of poly(butylene succinate) nanocompositescitations
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article
Effect of nanofiller's size and shape on the solid state microstructure and thermal properties of poly(butylene succinate) nanocomposites
Abstract
We report a study of the solid state microstructure and crystallization kinetics of poly(butylene succinate) (PBSu) reinforced with nanofillers of different shapes, sizes and geometries such as silver, silica (SiO 2 ), multi-walled carbon nanotubes (MWCNTs) and graphene oxide (GO). The solid state structure of neat polymer and nanocomposites were investigated by X-ray diffraction (XRD), polarized optical microscopy (POM) and transmission electron microscopy (TEM). The results indicated that the nanocomposite samples exhibited enhanced crystallinity and nucleation density, along with smaller spherulite size. Additionally, the spherical nanofillers were dispersed more uniformly in the polymeric matrix, than the other two filler types. The crystallization kinetics under both isothermal and dynamic conditions were also studied and as was expected, the nanocomposite samples, crystallize at higher rates due to the increased number of nucleation sites, as was calculated with Avrami, Dobreva and Friedman's methods. From the crystallization study it was found that the nanocomposite filled with Ag nanoparticles exhibited the highest rates from all other fillers followed from SiO 2 and MWCNTs while GO showed the lowest rates.