| People | Locations | Statistics |
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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Darr, Ja
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2020Tailoring the Charge/Discharge Potentials and Electrochemical Performance of SnO₂ Lithium‐Ion Anodes by Transition Metal Co‐Doping
- 2020Enhancing bifunctional catalytic activity of cobalt-nickel sulfide spinel nanocatalysts through transition metal doping and its application in secondary zinc-air batteries
- 2020Continuous Hydrothermal Synthesis of Metal Germanates (M₂GeO₄; M=Co, Mn, Zn) for High-Capacity Negative Electrodes in Li-Ion Batteries
- 2019Fabrication and characterisation of nanoscale Ni-CGO electrode from nanocomposite powders
- 2017Room temperature vanadium dioxide–carbon nanotube gas sensors made via continuous hydrothermal flow synthesis
- 2017Transparent conducting oxide thin films of Si-doped ZnO prepared by aerosol assisted CVD
- 2017Evaluating the Potential Benefits of Metal Ion Doping in SnO2 Negative Electrodes for Lithium Ion Batteries
- 2017High energy lithium ion battery electrode materials; enhanced charge storage via both alloying and insertion processes
- 2016Pilot-scale continuous synthesis of a vanadium-doped LiFePO4/C nanocomposite high-rate cathodes for lithium-ion batteries
- 2016Dispersion and microwave processing of nano-sized ITO powder for the fabrication of transparent conductive oxides
- 2014Imaging the continuous hydrothermal flow synthesis of nanoparticulate CeO2 at different supercritical water temperatures using in situ angle-dispersive diffractioncitations
- 2014Optical and photocatalytic behaviours of nanoparticles in the Ti-Zn-O binary systemcitations
- 2009Imaging the inside of a continuous nanoceramic synthesizer under supercritical water conditions using high-energy synchrotron x-radiationcitations
- 2007Preparation of polypropylene/sepiolite nanocomposites using supercritical CO2 assisted mixingcitations
Places of action
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article
Imaging the continuous hydrothermal flow synthesis of nanoparticulate CeO2 at different supercritical water temperatures using in situ angle-dispersive diffraction
Abstract
In situ high-energy synchrotron X-ray diffraction, a non-destructive synchrotron-based technique was employed to probe inside the steel tubing of a continuous hydrothermal flow synthesis (CHFS) mixer to spatially map, for the first time, the superheated water crystallisation of nanocrystalline ceria (CeO2) at three different (superheated-water) temperatures representing three unique chemical environments within the reactor. Rapid hydrothermal co-precipitation at the three selected temperatures led to similarly sized ceria nanoparticles ranging from 3 to 7 nm. 2D maps of CeO 2 formation were constructed from the intensity and corresponding full width at half maximum (FWHM) values of the two most intense ceria reflections (111) and (002) for all three water inlet temperatures (350, 400 and 450 C at 24 MPa) and subsequent changes in the particle size distribution were analysed. The accompanying high-resolution transmission electron microscopy (HRTEM) and tomographic particle size maps have confirmed that the mean ceria particle size slightly increases with temperature. This X-ray tomographic imaging study amounted to a formidable technical and engineering challenge, nevertheless one that has been met; this represents a significant achievement in imaging science, given the dynamic nature and hostile environment of a working CHFS reactor. © 2014 Elsevier B.V.