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| Naji, M. |
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| Motta, Antonella |
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| Aletan, Dirar |
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| Mohamed, Tarek |
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| Ertürk, Emre |
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| Taccardi, Nicola |
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| Kononenko, Denys |
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| Petrov, R. H. | Madrid |
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| Alshaaer, Mazen | Brussels |
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| Bih, L. |
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| Casati, R. |
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| Muller, Hermance |
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| Kočí, Jan | Prague |
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| Šuljagić, Marija |
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| Kalteremidou, Kalliopi-Artemi | Brussels |
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| Azam, Siraj |
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| Ospanova, Alyiya |
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| Blanpain, Bart |
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| Ali, M. A. |
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| Popa, V. |
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| Rančić, M. |
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| Ollier, Nadège |
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| Azevedo, Nuno Monteiro |
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| Landes, Michael |
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| Rignanese, Gian-Marco |
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Bensch, Wolfgang
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (21/21 displayed)
- 2023Directed Dehydration of Na$_4$Sn$_2$S$_6$ ⋅ 5H$_2$O Generates the New Compound Na$_4$Sn$_2$S$_6$: Crystal Structure and Selected Propertiescitations
- 2023Exfoliablity, magnetism, energy storage and stability of metal thiophosphate nanosheets made in liquid medium.citations
- 2022A Combined Sodium Intercalation and Copper Extrusion Mechanism in the Thiophosphate Family: CuCrP2S6 as Anode Material in Sodium‐Ion Batteriescitations
- 2022Time-dependent investigation of a mechanochemical synthesis of bismuth telluride-based materials and their structural and thermoelectric propertiescitations
- 2022Multi‐Method Characterization of the High‐Entropy Spinel Oxide $Mn_{0.2}Co_{0.2}Ni_{0.2}Cu_{0.2}Zn_{0.2}Fe_2O_4$ : Entropy Evidence, Microstructure, and Magnetic Propertiescitations
- 2021The Coordination Polymer Cr(en) 2 As 2 VO 7 Consisting of Alternating VO 4 Tetrahedra and As 2 O 5 Handles Decorated by Cr 3+ Centered Complexes
- 2020CuCo2S4 deposited on TiO2: Controlling the pH Value Boosts Photocatalytic Hydrogen Evolutioncitations
- 2019Nanostructured tungsten sulfides: insights into precursor decomposition and the microstructure using X-ray scattering methodscitations
- 2019High-Pressure Sintering of Rhombohedral Cr2S3 Using Titanium-Zirconium-Molybdenum Toolscitations
- 2019High‐Pressure Sintering of Rhombohedral Cr2S3 Using TZM Toolscitations
- 2019Hydrothermal Synthesis, Characterization, and Sintering Behavior of Core-Shell Particles: A Principle Study on Lanthanum Strontium Cobaltite Coated with Nanosized Gadolinium Doped Ceriacitations
- 2019Hydrothermal Synthesis, Characterization, and Sintering Behavior of Core-Shell Particles: A Principle Study on Lanthanum Strontium Cobaltite Coated with Nanosized Gadolinium Doped Ceriacitations
- 2018Transition metal cations on the move: simultaneous operando X-ray absorption spectroscopy and X-ray diffraction investigations during Li uptake and release of a $mathrm{NiFe_{2}O_{4}/CNT}$ compositecitations
- 2018Hydrothermal Synthesis, Characterization, and Sintering Behavior of Core-Shell Particles: A Principle Study on Lanthanum Strontium Cobaltite Coated with Nanosized Gadolinium Doped Ceriacitations
- 2016Nucleation and Crystal Growth of a $V_{14}Sb_{8}O_{42}$ Cluster from a $V_{15}Sb_{6}O_{42}$ Polyoxovanadate: In-Situ XRD Studiescitations
- 2016Nanostructure, thermoelectric properties, and transport theory of V2VI3 and V2VI3/IV-VI based superlattices and nanomaterialscitations
- 2014Synthesis and thermal instability of high-quality Bi2Te3/Sb2Te3 superlattice thin film thermoelectricscitations
- 2012Current Status in Fabrication, Structural and Transport Property Characterization, and Theoretical Understanding of Bi2Te3 / Sb2Te3 Superlattice Systemscitations
- 2008Investigation of SnSe, SnSe2, and Sn2Se3 alloys for phase change memory applicationscitations
- 2006[C3H10NO]2[Sb4S7]: Solvothermal syntheses, crystal structures and properties of the first thioantimonates containing aminoalcohols as structure directorscitations
- 2006A study of the reactivity of elemental Cr/Se/Te thin multilayers using X-ray reflectometry, in situ X-ray diffraction and X-ray absorption spectroscopycitations
Places of action
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article
[C3H10NO]2[Sb4S7]: Solvothermal syntheses, crystal structures and properties of the first thioantimonates containing aminoalcohols as structure directors
Abstract
Using solvothermal conditions two new thioantimonates with composition [C3H10NO]2[Sb4S7] were obtained containing protonated 1-amino-2-propanol as the structure directing molecule. Both compounds have the same composition but the anionic [Sb4S7]2- part is significantly different. In (1) three trigonal [SbS3] pyramids are connected via common corners yielding a [Sb3S6] ring. These rings are connected by another [SbS3] unit thus building the one-dimensional [Sb4S7]2- chain. In (2) a two dimensional [Sb4S7]2- anionic network is formed by the interconnection of two trigonal pyramidal [SbS3] units and two [SbS4] moieties. A remarkable feature of the structure is a [Sb4S10] moiety composed of four edge sharing [SbS4] units. The layered anion contains a Sb10S10 ring and the inter-layer distance of about 7.8 Å is caused by the special arrangement of the two crystallographically distinct protonated 1-amino-2-propanol cations. Both compounds were prepared using the same amount of starting materials but at different reaction temperatures. Hence, the two compounds are another examples for the sensitivity of reaction parameters in solvothermal syntheses. The compounds are optical semiconductors with band gaps of 2.10 eV (1) and 2.21 eV (2). Thermal decomposition in an inert atmosphere leads to a collapse of the structures and Sb2S3 is formed as the reaction product. © 2006 Elsevier SAS. All rights reserved.