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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Fernando, Gerard
University of Birmingham
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (22/22 displayed)
- 2023Effects of NaOH treatment and NaOH treatment conditions on the mechanical properties of coir fibres for use in composites manufacturecitations
- 2023Simultaneous multi-measurand analyses of cross-linking reactions within a differential scanning calorimeter using optical fibre sensorscitations
- 2023Single-Solvent Fractionation and Electro-Spinning Neat Softwood Kraft Lignincitations
- 2022Monitoring Cross-Linking, the Evolution of Refractive Index and the Glass Transition Temperature of an Epoxy Resin Using an Optical Fiber Sensorcitations
- 2021Vertically-aligned short E-glass fibre core sandwich composite: Production and evaluationcitations
- 2021Improved procedure for electro-spinning and carbonisation of neat solvent-fractionated softwood Kraft lignincitations
- 2016Monitoring pre-stressed composites using optical fibre sensorscitations
- 2016In-situ monitoring of cross-linking reactions using E-glass fibres and evanescent wave spectroscopycitations
- 2014Multi-point monitoring of cross-linking reactionscitations
- 2012Lateral spreading of a fiber bundle via mechanical meanscitations
- 2011Synthesis of Ag/AgCl-mesoporous silica nanocomposites using a simple aqueous solution-based chemical method and a study of their antibacterial activity on E. colicitations
- 2010Evaluation of Embedded Optical Fiber Composites: EFPI Sensor Response to Sensors in Fatigue Loadingcitations
- 2009In-situ damage detection using self-sensing compositescitations
- 2009Evaluation of embedded optical fiber sensors in composites: EFPI sensor fabrication and quasi-static evaluationcitations
- 2009A comparison of cure monitoring techniquescitations
- 2008A novel fibre optic acoustic emission sensorcitations
- 2008Chemical process monitoring and the detection of moisture ingress in composites - art. no. 69330R
- 2007Smart materials and systems
- 2007Fabrication of intrinsic fibre Fabry–Perot sensors in silica fibres using hydrofluoric acid etchingcitations
- 2006Process monitoring of fibre reinforced composites using optical fibre sensorscitations
- 2006Investigation of reversible photo-mechanical properties of azobenzene-based polymer films by nano-indentationcitations
- 2002A Method To Measure The Interfacial Shear Stress For Optical Fibres Embedded In Fibre Reinforced Composites
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article
Simultaneous multi-measurand analyses of cross-linking reactions within a differential scanning calorimeter using optical fibre sensors
Abstract
The cross-correlation of cross-linking kinetic data obtained from different analytical equipment is not straightforward because the experimental conditions are seldom identical (temperature gradient, mass of the sample and substrate containing the analyte). Furthermore, the measurement principles can also be different (thermal, optical, rheological, etc). This paper reports on the design and implementation of a multi-measurand fibre-optic probe within a differential scanning calorimeter. The probe consisted of two components: (i) a low-cost and disposable cleaved-end of an optical fibre that served as a Fresnel refection sensor; and (ii) an array of non-contact optical fibres that enabled FTIR spectra to be acquired from within the calorimeter. The Fresnel reflection sensor was used as an immersion device to infer the evolution of the refractive index during the cross-linking of an epoxy/amine thermosetting resin. The array of optical fibres enabled FTIR spectra to be acquired during the cross-linking of the thermosetting resin. The motivation for developing this capability was to demonstrate cross-correlation between the quantitative FTIR spectral data, the qualitative Fresnel reflection sensor and the output from the differential scanning calorimeter. The cross-linking kinetics were determined for the two optical techniques and an excellent correlation was found between them and the data obtained from the calorimeter. The feasibility of using the same Fresnel reflection sensor, after cross-lining of the resin, for detecting the glass transition temperature was demonstrated.