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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Pessanha, Sofia
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (13/13 displayed)
- 2023Maternal methylmercury exposure during early-life periods adversely affects mature enamel structure of offspring rats at human exposure levelscitations
- 2022Characterization of binders and pigments using an integrated analytical approach: Application to wooden reliefs created by Vasko Lipovac in the 1970scitations
- 2021Investigation of inks, pigments and paper in four Moroccan illuminated manuscripts dated to the eighteenth centurycitations
- 2020Evaluation of the effect of fluorinated tooth bleaching products using polarized Raman microscopy and particle induced gamma-ray emissioncitations
- 2019Josefa d' Óbidos workshop from panel to canvas. Multianalytical approach to materials and technical evolution of the most significant Portuguese painting workshop of the 17 th centurycitations
- 2016Distribution of toxic elements in teeth treated with amalgam using mu-energy dispersive X-ray fluorescencecitations
- 2016Jose de Escovar at the Chapel of the Souls: Technical and material study of a 1603 panel painting
- 2016Artificial aging paper to assess long-term effects of conservative treatment. Monitoring by infrared spectroscopy (ATR-FTIR), X-ray diffraction (XRD), and energy dispersive X-ray fluorescence (EDXRF)citations
- 2015Microscopy and X-Ray Spectroscopy Analyses for assessment gilding and silvering techniques of Portuguese illuminated manuscriptscitations
- 2015Nondestructive analysis of Portuguese “dinheiros” using XRF: overcoming patina constraintscitations
- 2009Comparison of matrix effects on portable and stationary XRF spectrometers for cultural heritage samplescitations
- 2009Efficacy of Waterborne Polyurethane to Prevent the Enzymatic Attack on Paper-Based Materialscitations
- 2008Analysis of a coloured Dutch map from the eighteenth centurycitations
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article
Evaluation of the effect of fluorinated tooth bleaching products using polarized Raman microscopy and particle induced gamma-ray emission
Abstract
In this in vitro study, the effect of the application of tooth bleaching products in human enamel was evaluated using polarized Raman microscopy, particle induced gamma-ray emission (PIGE) and Vickers Hardness test. Due to their acidic nature, teeth whitening products are associated with changes in enamel mineralization. Consequently, products have appeared in the market that promote the incorporation of fluorine in order to decrease the solubility of the hydroxyapatite in enamel and prevent demineralization. This way, four commercial products with different active principle concentrations: 16% carbamide peroxide (Opalescence PF (R) and VivaStyle (R)) or 6% hydrogen peroxide (Opalescence Go PF (R) and VivaStyle Paint On (R)) and presence or not of fluorine were compared. The information on the crystalline state of the enamel was provided by the determination of the depolarization ratio of the symmetric stretching band of phosphate (at 959 cm(-1)). Furthermore, the content and uptake of F was evaluated using PIGE in the two fluorinated products as well as in one negative control group. In order to evaluate the microhardness of enamel by means of Vickers test, another group of polished samples was prepared (using Opalescence PF (R)) and evaluated. Conversely to what could be expected, the obtained results determined a statistically significant decrease of depolarization ratio, leading to an increase of mineralization after the application of the bleaching products, except for VivaStyle (R). For this group, no significant variation was obtained before-after treatment, most likely due to the acidity of the product (pH=5.8). Additionally, an increase of concentration of F in the dental tissues was determined for the fluorinated products. On the other hand, enamel polishing, required for the application of the Vickers test, led to increased susceptibility to erosion, resulting in decreased hardness and an increased enamel depolarization rat(i)o.