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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Cardinaels, Ruth M.
KU Leuven
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (19/19 displayed)
- 2024Numerical simulation of fiber orientation kinetics and rheology of fiber-filled polymers in uniaxial extensioncitations
- 2024In situ experimental investigation of fiber orientation kinetics during uniaxial extensional flow of polymer compositescitations
- 2024A monolithic numerical model to predict the EMI shielding performance of lossy dielectric polymer nanocomposite shields in a rectangular waveguidecitations
- 2023A generalized mechano-statistical transient network model for unravelling the network topology and elasticity of hydrophobically associating multiblock copolymers in aqueous solutionscitations
- 2023Melt-Extruded Thermoplastic Liquid Crystal Elastomer Rotating Fiber Actuatorscitations
- 2023Melt-Extruded Thermoplastic Liquid Crystal Elastomer Rotating Fiber Actuatorscitations
- 2023Photoswitchable Liquid-to-Solid Transition of Azobenzene-Decorated Polysiloxanescitations
- 2022Laser sintering of PA12 particles studied by in-situ optical, thermal and X-ray characterizationcitations
- 2021Bio‐Based Poly(3‑hydroxybutyrate)/Thermoplastic Starch Composites as a Host Matrix for Biochar Fillerscitations
- 2020A filament stretching rheometer for in situ X-ray experimentscitations
- 2020Optimization of Anti-kinking Designs for Vascular Grafts Based on Supramolecular Materialscitations
- 2020Optimization of Anti-kinking Designs for Vascular Grafts Based on Supramolecular Materialscitations
- 2020Polymer spheres
- 2019A novel experimental setup for in-situ optical and X-ray imaging of laser sintering of polymer particlescitations
- 2019Laser sintering of polymer particle pairs studied by in-situ visualizationcitations
- 2018Thin film mechanical characterization of UV-curing acrylate systemscitations
- 2018Designing multi-layer polymeric nanocomposites for EM shielding in the X-bandcitations
- 2017Future nanocomposites : exploring multifunctional multi-layered architectures
- 2017Experimental setup for in situ visualization studies of laser sintering of polymer particles
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article
Thin film mechanical characterization of UV-curing acrylate systems
Abstract
This study presents the mechanical characterization of UV-curing acrylate systems. UV-curable polymers are commonly used in the stereolithography (SLA) technique to build multi-layered objects. Typically, the mechanical properties of the 3D-printed product are affected by the intrinsic material heterogeneity along the sample thickness. To understand what determines this heterogeneity, single layers of UV-curable polymer are characterized and the effect of process conditions on the mechanical properties is studied. Micro-compression experiments are carried out to determine the intrinsic mechanical properties which are representative of one single UV-cured layer. To determine the right conditions to generate maximally-cured micropillars, the evolution with irradiation time of monomer conversion, glass-transition temperature and yield stress has first been studied. Thereto, micrometer-sized pillars and dog-bone shaped samples have been prepared via UV-curing. Micro-compression measurements on maximally-cured micropillars are performed to study possible size effects. The results reveal that with decreasing pillar size, the yield stress decreases. Tensile measurements are performed on dog-bone shaped samples which have been processed in the same way as compared to the compression samples. These tensile tests show higher yield stress values when compared with compression tests. This size effect can be attributed to the rinsing with acetone during the sample preparation that leads to a removal of monomer from the crosslinked network. As a consequence, in the real 3D-printing process, the mechanical properties will depend on the feature size. In conclusion, a method is presented to determine the mechanical properties of one single layer of material used in the rapid-prototyping SLA process. The experimental procedure we adopted requires only a few millilitres of material and, therefore, is well suited for screening materials under real SLA process conditions.