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Drake, John E.
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Publications (3/3 displayed)
- 2009Synthesis and spectroscopic characterization of tris(O,O '-ditolyl dithiophosphato) arsenic/antimony/bismuth(III) compounds: Crystal structures of [As{S2P(OC6H4Me-m)2}3]·0.5C6H14, [Sb{S2P(OC6H4Me-m)2}3] and [Bi{S2P(OC6H4Me-m)2}3]citations
- 2009Synthesis and characterization of adducts of bis(O,O '-ditolyl/dibenzyl dithiophosphato)cobalt(II) with pyridine: Crystal structures of [Co{S2P(OC6H4Me-p)(2)}(2)(C5H5N)(2)] and [Co{S2P(OC6H4Me-p)(2)}(2)(NH3)]citations
- 2004New versatile phosphorus ligands containing SPNSO skeleton - synthesis and characterization of (SPPh2)(O2SR)NH acids (R = Me, C6H4Me-4) and their alkaline metal salts. Crystal and molecular structures of (SPPh2)(O2SR)NHcitations
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article
Synthesis and characterization of adducts of bis(O,O '-ditolyl/dibenzyl dithiophosphato)cobalt(II) with pyridine: Crystal structures of [Co{S2P(OC6H4Me-p)(2)}(2)(C5H5N)(2)] and [Co{S2P(OC6H4Me-p)(2)}(2)(NH3)]
Abstract
Bis(O,O'-ditolyl/dibenzyl dithiophosphato)cobalt(II) complexes with pyridine ligands of the type [Co{S2P(OR)(2)}(2)(C5H5N)(2)] (R = o-, m-, p-C6H4Me, CH2Ph) have been synthesized by the reaction of CoCl2(C5H5N)(2) and the corresponding ammonium salt of O,O'-ditolyl/dibenzyl dithiophosphate in methanol. These newly synthesized adducts were characterized by elemental analysis, IR, UV-Vis spectroscopy, magnetic susceptibility measurements and single crystal X-ray diffraction. These structures confirm that in the pyridine complex the geometry around the cobalt metal centre is distorted octahedral, and in the amine complex it is distorted trigonal bipyramidal.