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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Trager-Cowan, Carol
University of Strathclyde
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (25/25 displayed)
- 2022Structural and luminescence imaging and characterisation of semiconductors in the scanning electron microscope
- 2022Crystalline grain engineered CsPbIBr 2 films for indoor photovoltaicscitations
- 2022Crystalline grain engineered CsPbIBr2 films for indoor photovoltaicscitations
- 2020Structural and luminescence imaging and characterisation of semiconductors in the scanning electron microscopecitations
- 2020Nanomechanical behaviour of individual phases in WC-Co cemented carbides, from ambient to high temperaturecitations
- 2020Influence of micro-patterning of the growth template on defect reduction and optical properties of non-polar (112ˉ0) GaN
- 2020Metrology of crystal defects through intensity variations in secondary electrons from the diffraction of primary electrons in a scanning electron microscopecitations
- 2020Luminescence behavior of semipolar (10-11) InGaN/GaN "bow-tie" structures on patterned Si substratescitations
- 2020Influence of micro-patterning of the growth template on defect reduction and optical properties of non-polar (11-20) GaNcitations
- 2018Dislocation contrast in electron channelling contrast images as projections of strain-like componentscitations
- 2017Quantitative imaging of anti-phase domains by polarity sensitive orientation mapping using electron backscatter diffractioncitations
- 2017Quantitative imaging of anti-phase domains by polarity sensitive orientation mapping using electron backscatter diffractioncitations
- 2017Spatially-resolved optical and structural properties of semi-polar (11-22) AlxGa1-xN with x up to 0.56citations
- 2017Cross-correlation based high resolution electron backscatter diffraction and electron channelling contrast imaging for strain mapping and dislocation distributions in InAlN thin filmscitations
- 2017Exploring transmission Kikuchi diffraction using a Timepix detectorcitations
- 2016Reprint of
- 2016Optical and structural properties of GaN epitaxial layers on LiAlO2 substrates and their correlation with basal-plane stacking faultscitations
- 2016Electron channelling contrast imaging for III-nitride thin film structurescitations
- 2015Digital direct electron imaging of energy-filtered electron backscatter diffraction patternscitations
- 2013Electron channeling contrast imaging studies of nonpolar nitrides using a scanning electron microscopecitations
- 2012Imaging and identifying defects in nitride semiconductor thin films using a scanning electron microscopecitations
- 2008Rare earth doping of III-nitride alloys by ion implantationcitations
- 2004Development of CdSSe/CdS VCSELs for application to laser cathode ray tubes
- 2002Structural and optical properties of InGaN/GaN layers close to the critical layer thicknesscitations
- 2001Compositional pulling effects in InxGa1_xN/GaN layerscitations
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article
Nanomechanical behaviour of individual phases in WC-Co cemented carbides, from ambient to high temperature
Abstract
<p>The dependence of the mechanical behaviour of individual phases in WC-Co on microstructural parameters such as grain size and orientation were investigated by means of nanoindentation and electron microscopy. A broad range of WC grain dimensions, from about 1 to 1000 µm<sup>2</sup>, were selected and subsequently indented to investigate any size effect. A decrease in hardness as a function of grain dimensions was observed, due to an increase in dislocation mobility in larger grains. Whilst the binder phase only exhibits a hardness of about 11 GPa, the hardness of WC grains was measured about 29 and 53 GPa for the prismatic and basal orientations, respectively, in ambient conditions. All WC orientations exhibited a similar decrease in hardness with temperature, up to 700 ˚C. Damage mechanisms occurring in WC-Co during nanoindentation were investigated for the different grain orientations at various temperatures. The damage was visualised using electron microscopy near the residual indent coupled with Focused Ion Beam (FIB) sectioning across the indent. The three-dimensional distribution of plastic deformation across multiple grains in the vicinity of an indent was examined using Electron Channelling Contrast Imaging (ECCI). ECCI micrographs enabled the observation of crystal defects, especially dislocations, and slip lines as well as the entire plastic zone. The defect density and spatial distribution in the deformed WC grains were compared to that of an untested WC grain to identify the type of deformation originating from spherical indentation. The work provides important information on the relationship between WC-Co microstructure and performance at operating temperatures.</p>