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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Alfreider, Markus
Montanuniversität Leoben
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (21/21 displayed)
- 2024Stabilization of mechanical strength in a nanocrystalline CoCrNi concentrated alloy by nitrogen alloying
- 2024Micro-Mechanical Fracture Investigations on Grain Size Tailored Tungsten-Copper Nanocompositescitations
- 2024Automatic and time-resolved determination of fracture characteristics from in situ experimentscitations
- 2023Deformation and failure behavior of nanocrystalline WCucitations
- 2023Magnetic Properties of a High-Pressure Torsion Deformed Co-Zr Alloycitations
- 2023Revealing the nano-scale mechanisms of the limited non-basal plasticity in magnesium
- 2023Nanoscale printed tunable specimen geometry enables high-throughput miniaturized fracture testingcitations
- 2022In situ micromechanical analysis of a nano-crystalline W-Cu compositecitations
- 2022Interface mediated deformation and fracture of an elastic–plastic bimaterial system resolved by in situ transmission scanning electron microscopycitations
- 2022The influence of chemistry on the interface toughness in a WTi-Cu systemcitations
- 2021Prospects of Using Small Scale Testing to Examine Different Deformation Mechanisms in Nanoscale Single Crystals—A Case Study in Mgcitations
- 2021Extracting information from noisy data: strain mapping during dynamic in situ SEM experimentscitations
- 2020Correlation between fracture characteristics and valence electron concentration of sputtered Hf-C-N based thin filmscitations
- 2020In situ fracture observations of distinct interface types within a fully lamellar intermetallic TiAl alloycitations
- 2020Probing defect relaxation in ultra-fine grained Ta using micromechanical spectroscopycitations
- 2019Bioinspired nacre-like alumina with a bulk-metallic glass-forming alloy as a compliant phasecitations
- 2019Rate limiting deformation mechanisms of bcc metals in confined volumescitations
- 2018In-situ elastic-plastic fracture mechanics on the microscale by means of continuous dynamical testingcitations
- 2018In-situ TEM observation of {101¯2} twin-dominated deformation of Mg pillarscitations
- 2017The influence of deformation and proton-irradiation on the mechanical behaviour in nano-crystalline stainless steels
- 2016Synthesis and Mechanical Characterisation of an Ultra-Fine Grained Ti-Mg Compositecitations
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article
Deformation and failure behavior of nanocrystalline WCu
Abstract
The technical potential of WCu alloys is limited by the modest fracture characteristics of the material system in its coarse-grained condition. To provide a nanocrystalline microstructure and improve mechanical properties, a W-50 at.% Cu composite was processed using high-pressure torsion deformation at a temperature of 200 ◦C. Therefore, two specimens were subjected to 100% and 1000% shear strains, respectively. Scanning electron and scanning transmission electron microscopy, including nanoscale energy dispersive X-ray spectroscopy mappings, were used to quantify the resulting microstructures. The average grain sizes for the 100% and 1000% deformed specimens were determined to be 14.7 ± 6.6 nm and 10.5 ± 5.6 nm, with the amount of mechanically intermixed W in the Cu grains increasing from 15.4 at.% to 15.9 at.%. X-ray diffraction and selected area electron diffraction studies both revealed strained lattice parameters of the W and Cu phases, respectively. Mechanical properties were investigated using in-situ notched microcantilever tests. The mean conditional fracture toughness and J-integral values were comparable for both conditions, at 3.7 ± 0.4 MPa√m and 245 ± 58 J/m2, respectively. The related behavior could be attributed to the low fault tolerance of the highly deformed states and was substantiated by cleaved globular W grains along the fractured surfaces. In addition, the detailed relationship between the altered grain boundary conditions, the degree of mechanical intermixing and the influence of the different microstructures on the fracture properties were carefully evaluated and discussed to pave the way for future application of these high-strength nanocomposites.