• Leffers, T.
• Margulies, L.
• Martins, R. V.
• Poulsen, Henning, F.
• Schmidt, Søren

Abstract

First results are presented on the simultaneous observation of the elastic strain tensor as a function of load of 10 individual grains, deeply embedded in the bulk of a polycrystalline Al tensile sample. The experimental technique is based on the use of focused high energy synchrotron radiation in transmission geometry. After each load step diffraction patterns are collected with a large-area X-ray detector system for a series of different angular and lateral sample positions. An automated indexing routine was used to assign sets of diffraction spots to individual grains. The strain tensor components as well as the individual grain position within the sample were then fitted from the diffraction spot positions. A maximum tensile load of 48 MPa was applied. Deviations in strain of up to 600 × 10−6 are observed between respective strain components of individual grains.

Topics

• impedance spectroscopy
• grain
• x-ray diffraction