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Naji, M. |
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Motta, Antonella |
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Aletan, Dirar |
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Mohamed, Tarek |
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Ertürk, Emre |
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Taccardi, Nicola |
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Kononenko, Denys |
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Petrov, R. H. | Madrid |
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Alshaaer, Mazen | Brussels |
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Bih, L. |
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Casati, R. |
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Muller, Hermance |
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Kočí, Jan | Prague |
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Šuljagić, Marija |
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Kalteremidou, Kalliopi-Artemi | Brussels |
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Azam, Siraj |
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Ospanova, Alyiya |
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Blanpain, Bart |
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Ali, M. A. |
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Popa, V. |
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Rančić, M. |
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Ollier, Nadège |
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Azevedo, Nuno Monteiro |
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Landes, Michael |
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Rignanese, Gian-Marco |
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Zalesak, Jakub
University of Salzburg
in Cooperation with on an Cooperation-Score of 37%
Topics
Publications (14/14 displayed)
- 2024Backside metallization affects residual stress and bending strength of the recast layer in laser-diced Sicitations
- 2023W18O49 Nanowhiskers Decorating SiO2 Nanofiberscitations
- 2023Encapsulation of Uranium Oxide in Multiwall WS<sub>2</sub> Nanotubes
- 2023Mapping strain across Co80Ta7B13 / Co62Ta6B32 glassy interfaces
- 2023Probing the composition dependence of residual stress distribution in tungsten-titanium nanocrystalline thin filmscitations
- 2022Precipitation-based grain boundary design alters Inter- to Trans-granular Fracture in AlCrN Thin Filmscitations
- 2022Microstructure-dependent phase stability and precipitation kinetics in equiatomic CrMnFeCoNi high-entropy alloy: Role of grain boundariescitations
- 2021Powder Diffraction Data of Aluminum-Rich FCC-Ti1-xAlxN Prepared by CVDcitations
- 2020Nanoscale stress distributions and microstructural changes at scratch track cross-sections of a deformed brittle-ductile CrN-Cr bilayercitations
- 2020Evolution of stress fields during crack growth and arrest in a brittle-ductile CrN-Cr clamped-cantilever analysed by X-ray nanodiffraction and modellingcitations
- 2019Anisotropy of fracture toughness in nanostructured ceramics controlled by grain boundary designcitations
- 201830 nm X-ray focusing correlates oscillatory stress, texture and structural defect gradients across multilayered TiN-SiOx thin filmcitations
- 2017Peculiarity of self-assembled cubic nanolamellae in the TiN/AlN systemcitations
- 2016Combinatorial refinement of thin-film microstructure, properties and process conditions: iterative nanoscale search for self-assembled TiAlN nanolamellaecitations
Places of action
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article
Anisotropy of fracture toughness in nanostructured ceramics controlled by grain boundary design
Abstract
<p>The fracture toughness of nanostructured materials depends on anisotropic physical properties of individual microstructural features, their texture and/or topology. In this work, intentionally sculptured grain boundaries of low cohesive energy were used to form “weak” and “tough” crack propagation directions within a nanocrystalline TiN film, allowing to correlate the directional arrangement of grains and anisotropy of fracture toughness. By using a selective micromechanical testing approach, two different cracking directions were probed in a scanning electron microscope by loading microcantilever beam specimens prepared parallel and perpendicular to the stacked direction of the alternately tilted columnar grains. The fracture toughness along the sculptured grain boundaries was ~30% higher due to effective multiple crack deflection at the kink planes, which was not observed along weak cleavage planes in the stacked direction. The results indicate the fundamental importance of microstructural design in the synthesis of tough nanostructured ceramics, whose anisotropic mechanical properties can be controlled effectively by incorporating dedicated microstructural features of well-defined topology, orientation and density.</p>